Technology Process of C36H39BrN4O10S2
There total 8 articles about C36H39BrN4O10S2 which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
C26H29BrN2O6S;
With
trifluoroacetic acid;
for 1h;
2-Nitrobenzenesulfonyl chloride;
With
sodium hydrogencarbonate;
In
water; ethyl acetate;
(R)-2-(N-tert-butoxycarbonylamino)-3-buten-1-ol;
With
triphenylphosphine; diethylazodicarboxylate;
In
tetrahydrofuran; toluene;
at 0 - 20 ℃;
Further stages.;
DOI:10.1021/ja065724a
- Guidance literature:
-
Multi-step reaction with 5 steps
1.1: 45 percent / Amano Lipase PS from Pseudomonas cepacia / CH2Cl2 / 0.75 h
2.1: K2CO3 / methanol / 1 h
3.1: 81 percent / pyridine / 3 h
4.1: 99 percent / PPh3; diethyl azodicarboxylate / tetrahydrofuran; toluene / 0 - 20 °C
5.1: trifluoroacetic acid / 1 h
5.2: NaHCO3 / H2O; ethyl acetate
5.3: 93 percent / PPh3; diethyl azodicarboxylate / tetrahydrofuran; toluene / 0 - 20 °C
With
pyridine; potassium carbonate; triphenylphosphine; trifluoroacetic acid; diethylazodicarboxylate;
In
tetrahydrofuran; methanol; dichloromethane; toluene;
4.1: Fukuyama-Mitsunobu coupling reaction / 5.3: Fukuyama-Mitsunobu coupling reaction;
DOI:10.1021/ja065724a
- Guidance literature:
-
Multi-step reaction with 3 steps
1.1: 81 percent / pyridine / 3 h
2.1: 99 percent / PPh3; diethyl azodicarboxylate / tetrahydrofuran; toluene / 0 - 20 °C
3.1: trifluoroacetic acid / 1 h
3.2: NaHCO3 / H2O; ethyl acetate
3.3: 93 percent / PPh3; diethyl azodicarboxylate / tetrahydrofuran; toluene / 0 - 20 °C
With
pyridine; triphenylphosphine; trifluoroacetic acid; diethylazodicarboxylate;
In
tetrahydrofuran; toluene;
2.1: Fukuyama-Mitsunobu coupling reaction / 3.3: Fukuyama-Mitsunobu coupling reaction;
DOI:10.1021/ja065724a
