bromo(1,5,9-triazacyclododecane)zinc(II) bromide

Base Information

• Chemical Name: bromo(1,5,9-triazacyclododecane)zinc(II) bromide
• CAS No.: 113380-63-5
• Molecular Formula: Br*C₉H₂₁BrN₃Zn
• Molecular Weight: 396.484
• Mol file: 113380-63-5.mol

Synonyms:bromo(1,5,9-triazacyclododecane)zinc(II) bromide

Chemical Property of bromo(1,5,9-triazacyclododecane)zinc(II) bromide

Chemical Property:

Purity/Quality:

Safty Information:

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MSDS Files:

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Technology Process of bromo(1,5,9-triazacyclododecane)zinc(II) bromide

There total 1 articles about bromo(1,5,9-triazacyclododecane)zinc(II) bromide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

1,5,9,13,17,21-hexaazacyclotetracosane hexahydrobromide (113380-64-6) + 1,5,9-triazacyclododecane trihydrobromide (35980-62-2) + zinc dibromide (7699-45-8) → bromo(1,5,9-triazacyclododecane)zinc(II) bromide (113380-63-5)

Guidance literature:

With KOH; In ethanol; To a soln. of anhydrous ZnBr2 (abs. EtOH) a neutralized (gently heating to boiling, addn. of KOH, boiling with stirring for 15 min, allowing to cool to room temp., filtn.) mixt. of {12}aneN3*3HBr and {24}aneN6*6HBr in abs. EtOH is added dropwise.; Immediately a white ppt. forms, which is subsequently isolated by suction filtn., recrystn. from H2O, elem. anal.;

upstream raw materials:

1,5,9,13,17,21-hexaazacyclotetracosane hexahydrobromide

1,5,9-triazacyclododecane trihydrobromide

zinc dibromide