C₂₈H₁₈(OH)2(OSO₂C₆H₄CH₃)2(NHCOC₅H₄)2Co⁽¹⁺⁾*PF₆^(1-)=C₂₈H₁₈(OH)2(OSO₂C₆H₄CH₃)2(NHCOC₅H₄)2CoPF₆

Base Information

• Chemical Name: C₂₈H₁₈(OH)2(OSO₂C₆H₄CH₃)2(NHCOC₅H₄)2Co⁽¹⁺⁾*PF₆^(1-)=C₂₈H₁₈(OH)2(OSO₂C₆H₄CH₃)2(NHCOC₅H₄)2CoPF₆
• CAS No.: 187467-25-0
• Molecular Formula: C₅₄H₄₄CoN₂O₁₀S₂*F₆P
• Molecular Weight: 1149.04
• Mol file: 187467-25-0.mol

Synonyms:C₂₈H₁₈(OH)2(OSO₂C₆H₄CH₃)2(NHCOC₅H₄)2Co⁽¹⁺⁾*PF₆^(1-)=C₂₈H₁₈(OH)2(OSO₂C₆H₄CH₃)2(NHCOC₅H₄)2CoPF₆

Chemical Property of C₂₈H₁₈(OH)2(OSO₂C₆H₄CH₃)2(NHCOC₅H₄)2Co⁽¹⁺⁾*PF₆^(1-)=C₂₈H₁₈(OH)2(OSO₂C₆H₄CH₃)2(NHCOC₅H₄)2CoPF₆

Chemical Property:

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Technology Process of C₂₈H₁₈(OH)2(OSO₂C₆H₄CH₃)2(NHCOC₅H₄)2Co⁽¹⁺⁾*PF₆^(1-)=C₂₈H₁₈(OH)2(OSO₂C₆H₄CH₃)2(NHCOC₅H₄)2CoPF₆

There total 1 articles about C₂₈H₁₈(OH)2(OSO₂C₆H₄CH₃)2(NHCOC₅H₄)2Co⁽¹⁺⁾*PF₆^(1-)=C₂₈H₁₈(OH)2(OSO₂C₆H₄CH₃)2(NHCOC₅H₄)2CoPF₆ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 38.0%

ammonium hexafluorophosphate + 1,1'-bis(chlorocarbonyl)cobalticinium chloride + 5,17-diamino-25,27-dihydroxy-26,28-bis(tolylsulfonyloxy)calix[4]arene dihydrochloride → C28H18(OH)2(OSO2C6H4CH3)2(NHCOC5H4)2Co(1+)*PF6(1-)=C28H18(OH)2(OSO2C6H4CH3)2(NHCOC5H4)2CoPF6 (187467-25-0)

Guidance literature:

With NEt₃; In N,N-dimethyl-formamide; acetonitrile; N2-atmosphere; refluxing (1 h), evapn. (vac.); pptn. on H2O addn., drying (over P2O5), chromy. (SiO2, THF / MeCN / MeOH= 2 : 3 : 1), recrystn. (Me2CO); elem. anal.;

DOI:10.1021/om9904089