4-bromo-benzenesulfonic acid-(1-methyl-2-phenyl-ethyl ester)

Base Information

• Chemical Name: 4-bromo-benzenesulfonic acid-(1-methyl-2-phenyl-ethyl ester)
• CAS No.: 101352-92-5
• Molecular Formula: C₁₅H₁₅BrO₃S
• Molecular Weight: 355.252
• Mol file: 101352-92-5.mol

Synonyms:4-bromo-benzenesulfonic acid-(1-methyl-2-phenyl-ethyl ester)

Chemical Property of 4-bromo-benzenesulfonic acid-(1-methyl-2-phenyl-ethyl ester)

Chemical Property:

Purity/Quality:

Safty Information:

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MSDS Files:

Useful:

Technology Process of 4-bromo-benzenesulfonic acid-(1-methyl-2-phenyl-ethyl ester)

There total 2 articles about 4-bromo-benzenesulfonic acid-(1-methyl-2-phenyl-ethyl ester) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

4-bromo-benzenesulfonic acid-(2-phenyl-propyl ester) (855382-81-9) → 4-bromo-benzenesulfonic acid-(1-methyl-2-phenyl-ethyl ester) (101352-92-5)

Guidance literature:

Rate constant;

DOI:10.1021/ja01129a007

Reference yield:

→ 4-bromo-benzenesulfonic acid-(1-methyl-2-phenyl-ethyl ester) (101352-92-5)

Guidance literature:

/BRN= 2870736/;

DOI:10.1021/ja01125a007

Reference yield: 75.0%

ethyl N-diphenylmethylene glycine (69555-14-2) + 4-bromo-benzenesulfonic acid-(1-methyl-2-phenyl-ethyl ester) (101352-92-5) → C13H19NO2

Guidance literature:

ethyl N-diphenylmethylene glycine; 4-bromo-benzenesulfonic acid-(1-methyl-2-phenyl-ethyl ester); With potassium hexamethylsilazane; In toluene; at 40 ℃;

With hydrogenchloride; water; In 2-methyltetrahydrofuran; at 20 ℃; for 2h; diastereoselective reaction;

DOI:10.1021/acs.orglett.5b02448

upstream raw materials:

4-bromo-benzenesulfonic acid-(2-phenyl-propyl ester)