methyl 1-(1-(3-methoxyphenyl)-2-nitroethyl)-2-oxocyclopentanecarboxylate

Base Information

Chemical Name:methyl 1-(1-(3-methoxyphenyl)-2-nitroethyl)-2-oxocyclopentanecarboxylate
CAS No.:1092784-94-5
Molecular Formula:C₁₆H₁₉NO₆
Molecular Weight:321.33
Hs Code.:

Synonyms:methyl 1-(1-(3-methoxyphenyl)-2-nitroethyl)-2-oxocyclopentanecarboxylate

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Chemical Property of methyl 1-(1-(3-methoxyphenyl)-2-nitroethyl)-2-oxocyclopentanecarboxylate

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Technology Process of methyl 1-(1-(3-methoxyphenyl)-2-nitroethyl)-2-oxocyclopentanecarboxylate

There total 4 articles about methyl 1-(1-(3-methoxyphenyl)-2-nitroethyl)-2-oxocyclopentanecarboxylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 98.0%

: 3179-09-7,55446-68-9
(E)-1-methoxy-3-(2-nitrovinyl)benzene

: 10472-24-9,265317-94-0
methyl 2-oxocyclopentane-1-carboxylate

: 1092784-94-5
methyl 1-(1-(3-methoxyphenyl)-2-nitroethyl)-2-oxocyclopentanecarboxylate

Guidance literature:: With C₅₁H₄₂N₆; In toluene; at -10 ℃; for 31h; optical yield given as %ee; stereoselective reaction;
DOI:10.1016/j.tet.2011.05.005

Reference yield: 90.0%

: 3179-09-7
1-methoxy-3-(2-nitrovinyl)benzene

: 10472-24-9,265317-94-0
methyl 2-oxocyclopentane-1-carboxylate

: 1092784-94-5
methyl 1-(1-(3-methoxyphenyl)-2-nitroethyl)-2-oxocyclopentanecarboxylate

Guidance literature:: With 1-((1R,2R)-2-(dimethylamino)cyclohexyl)-3-((1R,2S)-2-hydroxy-1,2-diphenylethyl)thiourea; In dichloromethane; at -45 ℃; optical yield given as %ee; enantioselective reaction;
DOI:10.1002/chem.200801420

Reference yield:

: 3179-09-7,55446-68-9
(E)-1-methoxy-3-(2-nitrovinyl)benzene

: 10472-24-9,265317-94-0
methyl 2-oxocyclopentane-1-carboxylate

: methyl 1-(1-(3-methoxyphenyl)-2-nitroethyl)-2-oxocyclopentanecarboxylate

: 1092784-94-5
methyl 1-(1-(3-methoxyphenyl)-2-nitroethyl)-2-oxocyclopentanecarboxylate

: C₁₆H₁₉NO₆

Guidance literature:: With 1,2-O-isopropylidene-5-desoxy-5-N-tert-butylamino-α-D-xylofuranose; In isopropyl alcohol; at 20 ℃; for 24h; diastereoselective reaction;
DOI:10.3987/COM-19-14172