methyl 4-hydroxy-3-(2-methoxyethyl)-5-methylbenzoate

Base Information

Chemical Name:methyl 4-hydroxy-3-(2-methoxyethyl)-5-methylbenzoate
CAS No.:1031365-09-9
Molecular Formula:C₁₂H₁₆O₄
Molecular Weight:224.257
Hs Code.:

Synonyms:methyl 4-hydroxy-3-(2-methoxyethyl)-5-methylbenzoate

Suppliers and Price of methyl 4-hydroxy-3-(2-methoxyethyl)-5-methylbenzoate

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of methyl 4-hydroxy-3-(2-methoxyethyl)-5-methylbenzoate

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of methyl 4-hydroxy-3-(2-methoxyethyl)-5-methylbenzoate

There total 4 articles about methyl 4-hydroxy-3-(2-methoxyethyl)-5-methylbenzoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: C₁₈H₃₀O₄Si

: 1031365-09-9
methyl 4-hydroxy-3-(2-methoxyethyl)-5-methylbenzoate

Guidance literature:: With tetrabutyl ammonium fluoride; In tetrahydrofuran; at 20 ℃; for 0.0833333h;

Reference yield:

: 499-76-3
4-hydroxy-3-methylbenzoic acid

: 1031365-09-9
methyl 4-hydroxy-3-(2-methoxyethyl)-5-methylbenzoate

Guidance literature:: Multi-step reaction with 8 steps

1: thionyl chloride / 17 h / 0 - 20 °C / Inert atmosphere

2: potassium carbonate / acetone / 3 h / Reflux; Inert atmosphere

3: N,N-diethylaniline / 8 h / 200 °C / Inert atmosphere

4: triethylamine / dichloromethane / 72 h / 20 °C / Inert atmosphere

5: osmium(VIII) oxide; 2,6-dimethylpyridine; sodium periodate / 1,4-dioxane; water; acetone / 2 h / 20 °C / Inert atmosphere

6: sodium tetrahydroborate; methanol / 0.17 h / Cooling with ice

7: sodium hydrogencarbonate / dichloromethane / 16 h / 20 °C

8: tetrabutyl ammonium fluoride / tetrahydrofuran / 0.08 h / 20 °C

With 2,6-dimethylpyridine; methanol; sodium tetrahydroborate; sodium periodate; osmium(VIII) oxide; thionyl chloride; tetrabutyl ammonium fluoride; sodium hydrogencarbonate; potassium carbonate; triethylamine; N,N-diethylaniline; In tetrahydrofuran; 1,4-dioxane; dichloromethane; water; acetone;

Reference yield:

: 42113-13-3
methyl 4-hydroxy-3-methylbenzoate

: 1031365-09-9
methyl 4-hydroxy-3-(2-methoxyethyl)-5-methylbenzoate

Guidance literature:: Multi-step reaction with 7 steps

1: potassium carbonate / acetone / 3 h / Reflux; Inert atmosphere

2: N,N-diethylaniline / 8 h / 200 °C / Inert atmosphere

3: triethylamine / dichloromethane / 72 h / 20 °C / Inert atmosphere

4: osmium(VIII) oxide; 2,6-dimethylpyridine; sodium periodate / 1,4-dioxane; water; acetone / 2 h / 20 °C / Inert atmosphere

5: sodium tetrahydroborate; methanol / 0.17 h / Cooling with ice

6: sodium hydrogencarbonate / dichloromethane / 16 h / 20 °C

7: tetrabutyl ammonium fluoride / tetrahydrofuran / 0.08 h / 20 °C

With 2,6-dimethylpyridine; methanol; sodium tetrahydroborate; sodium periodate; osmium(VIII) oxide; tetrabutyl ammonium fluoride; sodium hydrogencarbonate; potassium carbonate; triethylamine; N,N-diethylaniline; In tetrahydrofuran; 1,4-dioxane; dichloromethane; water; acetone;