C₃₆H₅₀O₂₂

Base Information

• Chemical Name: C₃₆H₅₀O₂₂
• CAS No.: 676456-26-1
• Molecular Formula: C₃₆H₅₀O₂₂
• Molecular Weight: 834.78
• Mol file: 676456-26-1.mol

Synonyms:C₃₆H₅₀O₂₂

Chemical Property of C₃₆H₅₀O₂₂

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of C₃₆H₅₀O₂₂

There total 3 articles about C₃₆H₅₀O₂₂ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

C64H78O36 → C36H50O22 (676456-26-1)

Guidance literature:

With sodium methylate; In methanol; at 20 ℃; for 24h;

DOI:10.1039/b307802g

Reference yield:

para-diiodobenzene (624-38-4,1032416-46-8) → C36H50O22 (676456-26-1)

Guidance literature:

Multi-step reaction with 2 steps

1: 90 percent / Et₃N; CuI / Pd(Ph₃P)2Cl₂ / dimethylformamide / 5 h / 20 °C

2: 95 percent / NaOMe / methanol / 24 h / 20 °C

With copper(l) iodide; sodium methylate; triethylamine; bis-triphenylphosphine-palladium(II) chloride; In methanol; N,N-dimethyl-formamide; 1: Sonogashira coupling;

DOI:10.1039/b307802g

Reference yield:

propargyl 2,3,6-tri-O-acetyl-4-O-(2,3,4,6-tetra-O-acetyl-β-D-galactopyranosyl)-β-D-glucopyranoside (211688-85-6) → C36H50O22 (676456-26-1)

Guidance literature:

Multi-step reaction with 2 steps

1: 90 percent / Et₃N; CuI / Pd(Ph₃P)2Cl₂ / dimethylformamide / 5 h / 20 °C

2: 95 percent / NaOMe / methanol / 24 h / 20 °C

With copper(l) iodide; sodium methylate; triethylamine; bis-triphenylphosphine-palladium(II) chloride; In methanol; N,N-dimethyl-formamide; 1: Sonogashira coupling;

DOI:10.1039/b307802g

upstream raw materials:

para-diiodobenzene

propargyl 2,3,6-tri-O-acetyl-4-O-(2,3,4,6-tetra-O-acetyl-β-D-galactopyranosyl)-β-D-glucopyranoside