2'-(benzyloxycarbonyl)benzyl 2,3-di-O-benzoyl-6-O-benzyl-β-D-galactofuranoside

Base Information

Chemical Name:2'-(benzyloxycarbonyl)benzyl 2,3-di-O-benzoyl-6-O-benzyl-β-D-galactofuranoside
CAS No.:1033706-55-6
Molecular Formula:C₄₂H₃₈O₁₀
Molecular Weight:702.758
Hs Code.:

Synonyms:2'-(benzyloxycarbonyl)benzyl 2,3-di-O-benzoyl-6-O-benzyl-β-D-galactofuranoside

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Chemical Property of 2'-(benzyloxycarbonyl)benzyl 2,3-di-O-benzoyl-6-O-benzyl-β-D-galactofuranoside

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Technology Process of 2'-(benzyloxycarbonyl)benzyl 2,3-di-O-benzoyl-6-O-benzyl-β-D-galactofuranoside

There total 1 articles about 2'-(benzyloxycarbonyl)benzyl 2,3-di-O-benzoyl-6-O-benzyl-β-D-galactofuranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 86.0%

: 1033706-54-5
2'-(benzyloxycarbonyl)benzyl 2,3-di-O-benzoyl-β-D-galactofuranoside

: 100-44-7
benzyl chloride

: 1033706-55-6
2'-(benzyloxycarbonyl)benzyl 2,3-di-O-benzoyl-6-O-benzyl-β-D-galactofuranoside

Guidance literature:: 2'-(benzyloxycarbonyl)benzyl 2,3-di-O-benzoyl-β-D-galactofuranoside; In benzene; for 10h; Heating;

benzyl chloride; With tetra-(n-butyl)ammonium iodide; In N,N-dimethyl-formamide; at 60 ℃; for 3h; Further stages.;
DOI:10.1016/j.carres.2008.05.009

Reference yield: 92.0%

: 1033706-55-6
2'-(benzyloxycarbonyl)benzyl 2,3-di-O-benzoyl-6-O-benzyl-β-D-galactofuranoside

: 1033706-51-2
2'-carboxybenzyl 2,3,5-tri-O-benzoyl-6-O-t-butyldimethylsilyl-β-D-galactofuranoside

: 1033706-58-9
2'-(benzyloxycarbonyl)benzyl (2,3,5-tri-O-benzoyl-6-O-t-buthyldimethylsilyl-β-D-galactofuranosyl)-(1->5)-2,3-di-O-benzoyl-6-O-benzyl-β-D-galactofuranoside

Guidance literature:: 2'-(benzyloxycarbonyl)benzyl 2,3-di-O-benzoyl-6-O-benzyl-β-D-galactofuranoside; With 2,6-di-tert-butyl-4-methylpyridine; In dichloromethane; at 20 ℃; for 0.5h; Inert atmosphere; Molecular sieve;

2'-carboxybenzyl 2,3,5-tri-O-benzoyl-6-O-t-butyldimethylsilyl-β-D-galactofuranoside; With trifluoromethylsulfonic anhydride; In dichloromethane; at -78 - 0 ℃; Inert atmosphere;
DOI:10.1021/ol800530u

Reference yield: 88.0%

: 1033706-55-6
2'-(benzyloxycarbonyl)benzyl 2,3-di-O-benzoyl-6-O-benzyl-β-D-galactofuranoside

: 1046465-60-4
C₄₆H₃₈O₁₁

: 1046465-63-7
C₈₀H₆₈O₁₈

Guidance literature:: 2'-(benzyloxycarbonyl)benzyl 2,3-di-O-benzoyl-6-O-benzyl-β-D-galactofuranoside; With 2,6-di-tert-butyl-4-methylpyridine; In dichloromethane; at 20 ℃; for 0.166667h;

C₄₆H₃₈O₁₁; With trifluoromethylsulfonic anhydride; In dichloromethane; at -78 - 0 ℃; for 2h; Further stages.;
DOI:10.1016/j.carres.2008.05.009