O-Methoxymethyl mesembranol

Base Information

Chemical Name:O-Methoxymethyl mesembranol
CAS No.:156487-81-9
Molecular Formula:C₁₉H₂₉NO₄
Molecular Weight:335.444
Hs Code.:

Synonyms:O-Methoxymethyl mesembranol

Suppliers and Price of O-Methoxymethyl mesembranol

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Chemical Property of O-Methoxymethyl mesembranol

Chemical Property:

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Technology Process of O-Methoxymethyl mesembranol

There total 18 articles about O-Methoxymethyl mesembranol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 156487-79-5
2-<(1R,4R)-1-(3,4-Dimethoxyphenyl)-4-(methoxymethoxy)cyclohex-2-enyl>ethanal

: 156487-81-9
O-Methoxymethyl mesembranol

Guidance literature:: Multi-step reaction with 2 steps

1: 61 percent / NaBH₃CN, CH₃NH₂ / methanol / 24 h / Ambient temperature

2: 1.) Hg(OAc)2, 2.) NaBH₄, aq. NaOH / 1.) THF, r.t., 1 h, 2.) r.t.

With sodium hydroxide; sodium tetrahydroborate; mercury(II) diacetate; sodium cyanoborohydride; methylamine; In methanol;
DOI:10.1039/a604365h

Reference yield:

: 156487-78-4
Ethyl <(1R,4R)-1-(3,4-dimethoxyphenyl)-4-(methoxymethoxy)cyclohex-2-enyl>acetate

: 156487-81-9
O-Methoxymethyl mesembranol

Guidance literature:: Multi-step reaction with 3 steps

1: 82 percent / DIBALH / toluene / 0.25 h / -78 °C

2: 61 percent / NaBH₃CN, CH₃NH₂ / methanol / 24 h / Ambient temperature

3: 1.) Hg(OAc)2, 2.) NaBH₄, aq. NaOH / 1.) THF, r.t., 1 h, 2.) r.t.

With sodium hydroxide; sodium tetrahydroborate; mercury(II) diacetate; diisobutylaluminium hydride; sodium cyanoborohydride; methylamine; In methanol; toluene;
DOI:10.1039/a604365h

Reference yield:

: (R)-3-(3,4-Dimethoxy-phenyl)-6-methoxymethoxy-cyclohex-2-enol

: 156487-81-9
O-Methoxymethyl mesembranol

Guidance literature:: Multi-step reaction with 6 steps

1: 39 percent / pyridine / 12 h / Ambient temperature

2: 98 percent / K₂CO₃ / methanol / 1 h / Ambient temperature

3: 58 percent / molecular sieves 3 Angstroem, propionic acid / 48 h / 130 °C

4: 82 percent / DIBALH / toluene / 0.25 h / -78 °C

5: 61 percent / NaBH₃CN, CH₃NH₂ / methanol / 24 h / Ambient temperature

6: 1.) Hg(OAc)2, 2.) NaBH₄, aq. NaOH / 1.) THF, r.t., 1 h, 2.) r.t.

With pyridine; sodium hydroxide; sodium tetrahydroborate; 3 A molecular sieve; mercury(II) diacetate; diisobutylaluminium hydride; sodium cyanoborohydride; potassium carbonate; propionic acid; methylamine; In methanol; toluene;
DOI:10.1039/a604365h