(+/-)-16-oxa-14,15-dinor-13,16-inter-o-phenyleneleucotriene E₄ dimethyl ester

Base Information

Chemical Name:(+/-)-16-oxa-14,15-dinor-13,16-inter-o-phenyleneleucotriene E₄ dimethyl ester
CAS No.:109707-63-3
Molecular Formula:C₂₈H₄₁NO₆S
Molecular Weight:519.703
Hs Code.:

(+/-)-16-oxa-14,15-dinor-13,16-inter-o-phenyleneleucotriene E<sub>4</sub> dimethyl ester

Synonyms:(+/-)-16-oxa-14,15-dinor-13,16-inter-o-phenyleneleucotriene E₄ dimethyl ester

Suppliers and Price of (+/-)-16-oxa-14,15-dinor-13,16-inter-o-phenyleneleucotriene E₄ dimethyl ester

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (+/-)-16-oxa-14,15-dinor-13,16-inter-o-phenyleneleucotriene E₄ dimethyl ester

Chemical Property:

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Technology Process of (+/-)-16-oxa-14,15-dinor-13,16-inter-o-phenyleneleucotriene E₄ dimethyl ester

There total 6 articles about (+/-)-16-oxa-14,15-dinor-13,16-inter-o-phenyleneleucotriene E₄ dimethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 99.0%

: 18598-63-5
L-cysteine methyl ester hydrochloride

: 109707-62-2
(+/-)-16-oxa-14,15-dinor-13,16-inter-o-phenyleneleucotriene A₄ methyl ester

: 109707-63-3
(+/-)-16-oxa-14,15-dinor-13,16-inter-o-phenyleneleucotriene E₄ dimethyl ester

Guidance literature:: With triethylamine; In methanol; water; for 0.5h;

Reference yield:

: 107153-49-1
o-butoxyphenylethanol

: 109707-63-3
(+/-)-16-oxa-14,15-dinor-13,16-inter-o-phenyleneleucotriene E₄ dimethyl ester

Guidance literature:: Multi-step reaction with 4 steps

1: 65 percent / PBr₃, pyridine / diethyl ether / 1.) -30 deg C, 1 h; 2.) 20 deg C, 3 h

2: 4.13 g / acetonitrile / 144 h / Heating; sealed glass tube

3: 1.) butyllithium / 1.) THF, hexane, -78 deg C, 15 min; 2.) HMPTA, room temp.

4: 99 percent / triethylamine / methanol; H₂O / 0.5 h

With pyridine; n-butyllithium; phosphorus tribromide; triethylamine; In methanol; diethyl ether; water; acetonitrile;

Reference yield:

: 28456-81-7
o-butoxyallylbenzene

: 109707-63-3
(+/-)-16-oxa-14,15-dinor-13,16-inter-o-phenyleneleucotriene E₄ dimethyl ester

Guidance literature:: Multi-step reaction with 5 steps

1: 1.) ozone-oxygen; 2.) sodium borohydride / 1.) methanol, 10 deg C; 2.) room temp.

2: 65 percent / PBr₃, pyridine / diethyl ether / 1.) -30 deg C, 1 h; 2.) 20 deg C, 3 h

3: 4.13 g / acetonitrile / 144 h / Heating; sealed glass tube

4: 1.) butyllithium / 1.) THF, hexane, -78 deg C, 15 min; 2.) HMPTA, room temp.

5: 99 percent / triethylamine / methanol; H₂O / 0.5 h

With pyridine; sodium tetrahydroborate; n-butyllithium; oxygen; phosphorus tribromide; ozone; triethylamine; In methanol; diethyl ether; water; acetonitrile;