C₁₃H₁₃NO

Base Information

Chemical Name:C₁₃H₁₃NO
CAS No.:1350810-11-5
Molecular Formula:C₁₃H₁₃NO
Molecular Weight:199.252
Hs Code.:

Synonyms:C₁₃H₁₃NO

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Chemical Property of C₁₃H₁₃NO

Chemical Property:

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Technology Process of C₁₃H₁₃NO

There total 8 articles about C₁₃H₁₃NO which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 76.0%

: 1350810-10-4
C₂₀H₂₁NO₃S

: 1350810-11-5
C₁₃H₁₃NO

Guidance literature:: With 1,8-diazabicyclo[5.4.0]undec-7-ene; In tetrahydrofuran; at 20 ℃; for 16h;
DOI:10.1039/c1cc15257b

Reference yield:

: 1350810-01-3
C₂₁H₂₄N₂O₃S

: 1350810-11-5
C₁₃H₁₃NO

Guidance literature:: Multi-step reaction with 2 steps

1: hydrogenchloride; water / acetone / 70 °C

2: 1,8-diazabicyclo[5.4.0]undec-7-ene / tetrahydrofuran / 16 h / 20 °C

With hydrogenchloride; water; 1,8-diazabicyclo[5.4.0]undec-7-ene; In tetrahydrofuran; acetone;
DOI:10.1039/c1cc15257b

Reference yield:

: 1350810-16-0
C₁₈H₂₀INO₂S

: 1350810-11-5
C₁₃H₁₃NO

Guidance literature:: Multi-step reaction with 6 steps

1: potassium carbonate / acetone / Reflux

2: water; toluene-4-sulfonic acid / acetone / 80 °C

3: ethanol / 6 h / 20 °C

4: bis-triphenylphosphine-palladium(II) chloride; potassium carbonate; silver(l) oxide / toluene / 24 h / 120 °C / Inert atmosphere

5: hydrogenchloride; water / acetone / 70 °C

6: 1,8-diazabicyclo[5.4.0]undec-7-ene / tetrahydrofuran / 16 h / 20 °C

With hydrogenchloride; bis-triphenylphosphine-palladium(II) chloride; water; potassium carbonate; toluene-4-sulfonic acid; 1,8-diazabicyclo[5.4.0]undec-7-ene; silver(l) oxide; In tetrahydrofuran; ethanol; acetone; toluene; 4: Heck type reaction;
DOI:10.1039/c1cc15257b