C₂₆H₃₀N₂O

Base Information

Chemical Name:C₂₆H₃₀N₂O
CAS No.:1416772-52-5
Molecular Formula:C₂₆H₃₀N₂O
Molecular Weight:386.537
Hs Code.:

C<sub>26</sub>H<sub>30</sub>N<sub>2</sub>O

Synonyms:C₂₆H₃₀N₂O

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Chemical Property of C₂₆H₃₀N₂O

Chemical Property:

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Technology Process of C₂₆H₃₀N₂O

There total 9 articles about C₂₆H₃₀N₂O which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 67.0%

: 4784-77-4,29576-14-5,39616-19-8
(E/Z)-crotyl bromide

: 1416772-48-9
C₂₂H₂₂N₂O

: 1416772-52-5
C₂₆H₃₀N₂O

: C₂₆H₃₀N₂O

Guidance literature:: C₂₂H₂₂N₂O; With chromium dichloride; In tetrahydrofuran; at 200 ℃; for 0.416667h; Inert atmosphere; Schlenk technique;

(E/Z)-crotyl bromide; In tetrahydrofuran; at 20 ℃; for 3h; diastereoselective reaction;
DOI:10.1021/ml300385q

Reference yield:

: 1416772-49-0
C₂₃H₂₄N₂O₂

: 1416772-52-5
C₂₆H₃₀N₂O

: C₂₆H₃₀N₂O

Guidance literature:: Multi-step reaction with 3 steps

1.1: lithium aluminium tetrahydride / diethyl ether / 0.5 h / 0 °C / Inert atmosphere; Schlenk technique

2.1: Dess-Martin periodane / dichloromethane / 0.5 h / 0 °C / Inert atmosphere; Schlenk technique

3.1: chromium dichloride / tetrahydrofuran / 0.42 h / 200 °C / Inert atmosphere; Schlenk technique

3.2: 3 h / 20 °C

With chromium dichloride; lithium aluminium tetrahydride; Dess-Martin periodane; In tetrahydrofuran; diethyl ether; dichloromethane;
DOI:10.1021/ml300385q

Reference yield:

: 500-22-1
3-pyridinecarboxaldehyde

: 1416772-52-5
C₂₆H₃₀N₂O

: C₂₆H₃₀N₂O

Guidance literature:: Multi-step reaction with 8 steps

1.1: sodium acetate; acetic anhydride / 18 h / 115 °C / Inert atmosphere; Schlenk technique

2.1: sodium acetate / 72 h / 20 °C / Inert atmosphere; Schlenk technique

3.1: tetrafluoroboric acid; (R,R)-(-)-1,2-bis[(o-methoxyphenyl)(phenyl) phosphino]ethane(1,5-cyclooctadiene)rhodium(I) tetrafluoroborate; hydrogen / methanol / 18 h / 50 °C / 3750.38 Torr / Autoclave; Schlenk technique

4.1: thionyl chloride / methanol / 18 h / 0 - 80 °C / Inert atmosphere; Schlenk technique

5.1: sodium cyanoborohydride; acetic acid / methanol / 24 h / 20 °C / Molecular sieve; Inert atmosphere; Schlenk technique

6.1: lithium aluminium tetrahydride / diethyl ether / 0.5 h / 0 °C / Inert atmosphere; Schlenk technique

7.1: Dess-Martin periodane / dichloromethane / 0.5 h / 0 °C / Inert atmosphere; Schlenk technique

8.1: chromium dichloride / tetrahydrofuran / 0.42 h / 200 °C / Inert atmosphere; Schlenk technique

8.2: 3 h / 20 °C

With chromium dichloride; lithium aluminium tetrahydride; tetrafluoroboric acid; thionyl chloride; (R,R)-(-)-1,2-bis[(o-methoxyphenyl)(phenyl) phosphino]ethane(1,5-cyclooctadiene)rhodium(I) tetrafluoroborate; hydrogen; sodium acetate; acetic anhydride; sodium cyanoborohydride; Dess-Martin periodane; acetic acid; In tetrahydrofuran; methanol; diethyl ether; dichloromethane;
DOI:10.1021/ml300385q