benzyl 3-O-benzyl-4,6-O-benzylidene-β-D-mannopyranosyl-(1->2)-3-O-benzyl-4,6-O-benzylidene-α-D-mannopyranoside

Base Information

• Chemical Name: benzyl 3-O-benzyl-4,6-O-benzylidene-β-D-mannopyranosyl-(1->2)-3-O-benzyl-4,6-O-benzylidene-α-D-mannopyranoside
• CAS No.: 1145656-15-0
• Molecular Formula: C₄₇H₄₈O₁₁
• Molecular Weight: 788.892

Synonyms:benzyl 3-O-benzyl-4,6-O-benzylidene-β-D-mannopyranosyl-(1->2)-3-O-benzyl-4,6-O-benzylidene-α-D-mannopyranoside

Chemical Property of benzyl 3-O-benzyl-4,6-O-benzylidene-β-D-mannopyranosyl-(1->2)-3-O-benzyl-4,6-O-benzylidene-α-D-mannopyranoside

Chemical Property:

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Technology Process of benzyl 3-O-benzyl-4,6-O-benzylidene-β-D-mannopyranosyl-(1->2)-3-O-benzyl-4,6-O-benzylidene-α-D-mannopyranoside

There total 1 articles about benzyl 3-O-benzyl-4,6-O-benzylidene-β-D-mannopyranosyl-(1->2)-3-O-benzyl-4,6-O-benzylidene-α-D-mannopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

C50H50O11 → benzyl 3-O-benzyl-4,6-O-benzylidene-β-D-mannopyranosyl-(1->2)-3-O-benzyl-4,6-O-benzylidene-α-D-mannopyranoside (1145656-15-0)

Guidance literature:

With osmium(VIII) oxide; 4-methylmorpholine N-oxide; In water; acetonitrile; at 20 ℃; for 2.5h;

DOI:10.1002/ejoc.200801024

Reference yield:

benzyl 3-O-benzyl-4,6-O-benzylidene-β-D-mannopyranosyl-(1->2)-3-O-benzyl-4,6-O-benzylidene-α-D-mannopyranoside (1145656-15-0) → C19H34O11 + β-D-mannopyranosyl-(1->2)-D-mannopyranoside (50271-63-1) + β-D-mannopyranosyl-(1->2)-D-mannopyranoside (50271-58-4)

Guidance literature:

With palladium on activated charcoal; hydrogen; In methanol; water; at 20 ℃; for 16h; under 2587.76 Torr; optical yield given as %de;

DOI:10.1002/ejoc.200801024

Reference yield:

C24H23F3O8S + benzyl 3-O-benzyl-4,6-O-benzylidene-β-D-mannopyranosyl-(1->2)-3-O-benzyl-4,6-O-benzylidene-α-D-mannopyranoside (1145656-15-0) → benzyl 3-O-benzyl-4,6-O-benzylidene-2-O-(prop-2-ynyl)-β-D-mannopyranosyl-(1->2)-3-O-benzyl-4,6-O-benzylidene-β-D-mannopyranosyl-(1->2)-3-O-benzyl-4,6-O-benzylidene-α-D-mannopyranoside (1144104-18-6) + C70H70O16

Guidance literature:

In dichloromethane; at -78 ℃; for 2h; optical yield given as %de; Inert atmosphere;

DOI:10.1002/ejoc.200801024

Downstream raw materials:

benzyl 3-O-benzyl-4,6-O-benzylidene-2-O-(prop-2-ynyl)-β-D-mannopyranosyl-(1->2)-3-O-benzyl-4,6-O-benzylidene-β-D-mannopyranosyl-(1->2)-3-O-benzyl-4,6-O-benzylidene-α-D-mannopyranoside

β-D-mannopyranosyl-(1->2)-D-mannopyranoside

β-D-mannopyranosyl-(1->2)-D-mannopyranoside

benzyl 2,3-di-O-benzyl-4,6-O-benzylidene-β-D-mannopyranosyl-(1->2)-3-O-benzyl-4,6-O-benzylidene-β-D-mannopyranosyl-(1->2)-3-O-benzyl-4,6-O-benzylidene-β-D-mannopyranosyl-(1->2)-3-O-benzyl-4,6-O-benzylidene-α-D-mannopyranoside

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