2,3,4,6-tetra-O-benzoyl-β-D-galactopyranose-(1->3)-1,2-O-isopropylidene-β-D-xylose

Base Information

Chemical Name:2,3,4,6-tetra-O-benzoyl-β-D-galactopyranose-(1->3)-1,2-O-isopropylidene-β-D-xylose
CAS No.:1272617-06-7
Molecular Formula:C₄₂H₄₀O₁₄
Molecular Weight:768.771
Hs Code.:

Synonyms:2,3,4,6-tetra-O-benzoyl-β-D-galactopyranose-(1->3)-1,2-O-isopropylidene-β-D-xylose

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Chemical Property of 2,3,4,6-tetra-O-benzoyl-β-D-galactopyranose-(1->3)-1,2-O-isopropylidene-β-D-xylose

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Technology Process of 2,3,4,6-tetra-O-benzoyl-β-D-galactopyranose-(1->3)-1,2-O-isopropylidene-β-D-xylose

There total 5 articles about 2,3,4,6-tetra-O-benzoyl-β-D-galactopyranose-(1->3)-1,2-O-isopropylidene-β-D-xylose which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 96.0%

: 1272617-04-5
2,3,4,6-tetra-O-benzoyl-β-D-galactopyranose-(1->3)-5-aldehyde-1,2-O-isopropylidene-α-D-glucofuranose

: 1272617-06-7
2,3,4,6-tetra-O-benzoyl-β-D-galactopyranose-(1->3)-1,2-O-isopropylidene-β-D-xylose

Guidance literature:: With sodium tetrahydroborate; In water; ethyl acetate; at 0 ℃; for 0.25h;
DOI:10.3390/molecules16021113

Reference yield:

: 844699-62-3
2,3,4,6-tetra-O-benzoyl-β-D-galactopyranosyl-(1->3)-1,2-O-isopropylidene-α-D-glucofuranose

: 1272617-06-7
2,3,4,6-tetra-O-benzoyl-β-D-galactopyranose-(1->3)-1,2-O-isopropylidene-β-D-xylose

Guidance literature:: Multi-step reaction with 2 steps

1: silicagel supported NaIO₄ / dichloromethane / 0.42 h / 20 °C

2: sodium tetrahydroborate / water; ethyl acetate / 0.25 h / 0 °C

With sodium tetrahydroborate; In dichloromethane; water; ethyl acetate;
DOI:10.3390/molecules16021113

Reference yield:

: 2,3,4,6-tetra-O-benzoyl-β-D-galactopyranosyl-(1->3)-1,2:5,6-di-O-isopropylidene-α-D-glucofuranose

: 1272617-06-7
2,3,4,6-tetra-O-benzoyl-β-D-galactopyranose-(1->3)-1,2-O-isopropylidene-β-D-xylose

Guidance literature:: Multi-step reaction with 3 steps

1: acetic acid / 6 h / 25 °C

2: silicagel supported NaIO₄ / dichloromethane / 0.42 h / 20 °C

3: sodium tetrahydroborate / water; ethyl acetate / 0.25 h / 0 °C

With sodium tetrahydroborate; acetic acid; In dichloromethane; water; ethyl acetate;
DOI:10.3390/molecules16021113