Technology Process of C51H80N2O25
There total 5 articles about C51H80N2O25 which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
ammonium cerium(IV) nitrate; borate buffer;
In
acetonitrile;
at 50 ℃;
for 2h;
DOI:10.1021/jo035329s
- Guidance literature:
-
Multi-step reaction with 3 steps
1: 86 percent / 4-(dimethylamino)pyridine; (diisopropyl)ethylamine / benzene / 0.5 h / 20 °C
2: 91 percent / 4-(dimethylamino)pyridinium p-toluenesulfonate; 4-(dimethylamino)pyridine; N,N'-dicyclohexylcarbodiimide / CH2Cl2 / 20 °C
3: 85 percent / borate buffer; ceric ammonium nitrate / acetonitrile / 2 h / 50 °C
With
dmap; ammonium cerium(IV) nitrate; borate buffer; N-ethyl-N,N-diisopropylamine; dicyclohexyl-carbodiimide; 4-(dimethylamino)pyridinium tosylate;
In
dichloromethane; acetonitrile; benzene;
DOI:10.1021/jo035329s
- Guidance literature:
-
Multi-step reaction with 4 steps
1: 65 percent / pyridine / CH2Cl2 / 0.17 h / 0 °C
2: 86 percent / 4-(dimethylamino)pyridine; (diisopropyl)ethylamine / benzene / 0.5 h / 20 °C
3: 91 percent / 4-(dimethylamino)pyridinium p-toluenesulfonate; 4-(dimethylamino)pyridine; N,N'-dicyclohexylcarbodiimide / CH2Cl2 / 20 °C
4: 85 percent / borate buffer; ceric ammonium nitrate / acetonitrile / 2 h / 50 °C
With
pyridine; dmap; ammonium cerium(IV) nitrate; borate buffer; N-ethyl-N,N-diisopropylamine; dicyclohexyl-carbodiimide; 4-(dimethylamino)pyridinium tosylate;
In
dichloromethane; acetonitrile; benzene;
DOI:10.1021/jo035329s