(4-Amino-3-nitro-phenyl)-phosphoramidic acid bis-(4-chloro-phenyl) ester

Base Information

Chemical Name:(4-Amino-3-nitro-phenyl)-phosphoramidic acid bis-(4-chloro-phenyl) ester
CAS No.:115752-40-4
Molecular Formula:C₁₈H₁₄Cl₂N₃O₅P
Molecular Weight:454.206
Hs Code.:

Synonyms:(4-Amino-3-nitro-phenyl)-phosphoramidic acid bis-(4-chloro-phenyl) ester

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Chemical Property of (4-Amino-3-nitro-phenyl)-phosphoramidic acid bis-(4-chloro-phenyl) ester

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Technology Process of (4-Amino-3-nitro-phenyl)-phosphoramidic acid bis-(4-chloro-phenyl) ester

There total 1 articles about (4-Amino-3-nitro-phenyl)-phosphoramidic acid bis-(4-chloro-phenyl) ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 52.0%

: 5307-14-2,183870-67-9
2-nitro-1,4-phenylenediamine

: 15074-53-0
bis(4-chlorophenyl)phosphoryl chloride

: 115752-40-4
(4-Amino-3-nitro-phenyl)-phosphoramidic acid bis-(4-chloro-phenyl) ester

Guidance literature:: With triethylamine; In 1,4-dioxane; at 80 ℃; for 12h;

Reference yield:

: 115752-40-4
(4-Amino-3-nitro-phenyl)-phosphoramidic acid bis-(4-chloro-phenyl) ester

: (3,4-Diamino-phenyl)-phosphoramidic acid bis-(4-chloro-phenyl) ester

Guidance literature:: With hydrogen; palladium on activated charcoal; In methanol;

Reference yield:

: 115752-40-4
(4-Amino-3-nitro-phenyl)-phosphoramidic acid bis-(4-chloro-phenyl) ester

: 115752-29-9
{5-[Bis-(4-chloro-phenoxy)-phosphorylamino]-1H-benzoimidazol-2-yl}-carbamic acid methyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: H₂ / 10 percent Pd/C / methanol

2: 25 percent / p-toluenesulfonic acid / methanol / 3 h / Heating

With hydrogen; toluene-4-sulfonic acid; palladium on activated charcoal; In methanol;