6-(7-Methoxy-2,2-dimethyl-3-phenyl-2H-chromen-4-yl)-4-propyl-3,4-dihydro-2H-benzo[1,4]oxazine

Base Information

Chemical Name:6-(7-Methoxy-2,2-dimethyl-3-phenyl-2H-chromen-4-yl)-4-propyl-3,4-dihydro-2H-benzo[1,4]oxazine
CAS No.:78838-60-5
Molecular Formula:C₂₉H₃₁NO₃
Molecular Weight:441.57
Hs Code.:

Synonyms:6-(7-Methoxy-2,2-dimethyl-3-phenyl-2H-chromen-4-yl)-4-propyl-3,4-dihydro-2H-benzo[1,4]oxazine

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Chemical Property of 6-(7-Methoxy-2,2-dimethyl-3-phenyl-2H-chromen-4-yl)-4-propyl-3,4-dihydro-2H-benzo[1,4]oxazine

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Technology Process of 6-(7-Methoxy-2,2-dimethyl-3-phenyl-2H-chromen-4-yl)-4-propyl-3,4-dihydro-2H-benzo[1,4]oxazine

There total 5 articles about 6-(7-Methoxy-2,2-dimethyl-3-phenyl-2H-chromen-4-yl)-4-propyl-3,4-dihydro-2H-benzo[1,4]oxazine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 75.0%

: 78838-55-8
6-<4'-(7'-Methoxy-2',2'-dimethyl-3'-phenyl)chromenyl>dihydrobenz-1,4-oxazine

: 78838-60-5
6-(7-Methoxy-2,2-dimethyl-3-phenyl-2H-chromen-4-yl)-4-propyl-3,4-dihydro-2H-benzo[1,4]oxazine

Guidance literature:: With potassium carbonate; In N,N-dimethyl-formamide; for 24h; Ambient temperature;

Reference yield:

: 51423-23-5
4-(4-hydroxyphenyl)-7-methoxy-2,2-dimethyl-3-phenyl-2H-benzopyran

: 78838-60-5
6-(7-Methoxy-2,2-dimethyl-3-phenyl-2H-chromen-4-yl)-4-propyl-3,4-dihydro-2H-benzo[1,4]oxazine

Guidance literature:: Multi-step reaction with 5 steps

1: 80 percent

2: 95 percent / K₂CO₃ / acetone / Heating

3: 100 percent / H₂ / Raney-Ni / methanol / 23 h / Ambient temperature

4: 96 percent / LAH / diethyl ether; tetrahydrofuran / in the cold

5: 75 percent / K₂CO₃ / dimethylformamide / 24 h / Ambient temperature

With lithium aluminium tetrahydride; hydrogen; potassium carbonate; nickel; In tetrahydrofuran; methanol; diethyl ether; N,N-dimethyl-formamide; acetone;

Reference yield:

: 71855-97-5
4-(7-Methoxy-2,2-dimethyl-3-phenyl-2H-chromen-4-yl)-2-nitro-phenol

: 78838-60-5
6-(7-Methoxy-2,2-dimethyl-3-phenyl-2H-chromen-4-yl)-4-propyl-3,4-dihydro-2H-benzo[1,4]oxazine

Guidance literature:: Multi-step reaction with 4 steps

1: 95 percent / K₂CO₃ / acetone / Heating

2: 100 percent / H₂ / Raney-Ni / methanol / 23 h / Ambient temperature

3: 96 percent / LAH / diethyl ether; tetrahydrofuran / in the cold

4: 75 percent / K₂CO₃ / dimethylformamide / 24 h / Ambient temperature

With lithium aluminium tetrahydride; hydrogen; potassium carbonate; nickel; In tetrahydrofuran; methanol; diethyl ether; N,N-dimethyl-formamide; acetone;