1-[(4-Methylphenyl)sulfonyl]azetidin-3-one oxime

Base Information

Chemical Name:1-[(4-Methylphenyl)sulfonyl]azetidin-3-one oxime
CAS No.:154010-97-6
Molecular Formula:C₁₀H₁₂N₂O₃S
Molecular Weight:240.283
Hs Code.:
DSSTox Substance ID:DTXSID101238843
Nikkaji Number:J652.724H
ChEMBL ID:CHEMBL1385728

Synonyms:Oprea1_754334;SCHEMBL1098149;CHEMBL1385728;DTXSID101238843;HMS2415O07;3-oximino-1-(p-toluenesulfonyl)azetidine;1-[(4-Methylphenyl)sulfonyl]-3-azetidinone oxime;1-[(4-Methylphenyl)sulfonyl]azetidin-3-one oxime;154010-97-6

Suppliers and Price of 1-[(4-Methylphenyl)sulfonyl]azetidin-3-one oxime

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

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Total 0 raw suppliers

Chemical Property of 1-[(4-Methylphenyl)sulfonyl]azetidin-3-one oxime

Chemical Property:

XLogP3:1.3
Hydrogen Bond Donor Count:1
Hydrogen Bond Acceptor Count:5
Rotatable Bond Count:2
Exact Mass:240.05686342
Heavy Atom Count:16
Complexity:369

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Canonical SMILES:CC1=CC=C(C=C1)S(=O)(=O)N2CC(=NO)C2

Technology Process of 1-[(4-Methylphenyl)sulfonyl]azetidin-3-one oxime

There total 9 articles about 1-[(4-Methylphenyl)sulfonyl]azetidin-3-one oxime which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

: 76543-27-6
1-(p-toluenesulfonyl) azetidin-3-one

: 154010-97-6
3-oximino-1-(p-toluenesulfonyl) azetidine

Guidance literature:: With hydroxylamine hydrochloride; sodium acetate; In methanol; for 2h; Reflux;
DOI:10.1007/s11172-009-0277-y

Reference yield:

: 154010-96-5
1-(p-Toluenesulfonyl)azetidin-3-ol

: 154010-97-6
3-oximino-1-(p-toluenesulfonyl) azetidine

Guidance literature:: Multi-step reaction with 2 steps

1: 94 percent / 2-iodoxybenzoic acid / ethyl acetate / 20 h / Heating

2: 90 percent / sodium acetate trihydrate; hydroxylamine hydrochloride / methanol / 2 h / Heating

With hydroxylamine hydrochloride; sodium acetate; 1-hydroxy-3H-benz[d][1,2]iodoxole-1,3-dione; In methanol; ethyl acetate;

Reference yield:

: 72676-71-2
N-(3-Diazo-2-oxo-propyl)-4-methyl-benzenesulfonamide

: 154010-97-6
3-oximino-1-(p-toluenesulfonyl) azetidine

Guidance literature:: Multi-step reaction with 2 steps

1: bis(hexafluoroacetylacetonato)copper(II)

2: 90 percent / NaOAc*3H₂O, NH₂OH*HCl / methanol / 2 h / Heating

With hydroxylamine hydrochloride; sodium acetate; copper(II) hexafluoro-2,4-pentanedionate; In methanol;
DOI:10.1021/jo00112a014