2-methyl-5-{2-methyl-6-[(3-methyl-2,5-dioxo-2,5-dihydro-1H-pyrrol-1yl)amino]pyrimidin-4-yl}benzenesulphonamide

Base Information

Chemical Name:2-methyl-5-{2-methyl-6-[(3-methyl-2,5-dioxo-2,5-dihydro-1H-pyrrol-1yl)amino]pyrimidin-4-yl}benzenesulphonamide
CAS No.:1055923-52-8
Molecular Formula:C₁₇H₁₇N₅O₄S
Molecular Weight:387.419
Hs Code.:

Synonyms:2-methyl-5-{2-methyl-6-[(3-methyl-2,5-dioxo-2,5-dihydro-1H-pyrrol-1yl)amino]pyrimidin-4-yl}benzenesulphonamide

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Chemical Property of 2-methyl-5-{2-methyl-6-[(3-methyl-2,5-dioxo-2,5-dihydro-1H-pyrrol-1yl)amino]pyrimidin-4-yl}benzenesulphonamide

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Technology Process of 2-methyl-5-{2-methyl-6-[(3-methyl-2,5-dioxo-2,5-dihydro-1H-pyrrol-1yl)amino]pyrimidin-4-yl}benzenesulphonamide

There total 6 articles about 2-methyl-5-{2-methyl-6-[(3-methyl-2,5-dioxo-2,5-dihydro-1H-pyrrol-1yl)amino]pyrimidin-4-yl}benzenesulphonamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 616-02-4
citraconic acid anhydride

: 1055923-54-0
5-(6-hydrazino-2-methylpyrimidin-4-yl)-2-methyl benzenesulphonamide

: 1055923-52-8
2-methyl-5-{2-methyl-6-[(3-methyl-2,5-dioxo-2,5-dihydro-1H-pyrrol-1yl)amino]pyrimidin-4-yl}benzenesulphonamide

Guidance literature:: In methanol; chloroform; at 80 ℃; for 4h; Heating / reflux;

Reference yield:

: C₁₂H₁₀Cl₂N₂O₂S

: 1055923-52-8
2-methyl-5-{2-methyl-6-[(3-methyl-2,5-dioxo-2,5-dihydro-1H-pyrrol-1yl)amino]pyrimidin-4-yl}benzenesulphonamide

Guidance literature:: Multi-step reaction with 3 steps

1: ammonia / dichloromethane / 0.33 h / 5 - 20 °C

2: hydrazine / tetrahydrofuran / 6 h / 70 °C / Heating / reflux

3: methanol; chloroform / 4 h / 80 °C / Heating / reflux

With ammonia; hydrazine; In tetrahydrofuran; methanol; dichloromethane; chloroform;

Reference yield:

: 1055923-53-9
5-(6-chloro-2-methylpyrimidin-4-yl)-2-methylbenzene sulphonamide

: 1055923-52-8
2-methyl-5-{2-methyl-6-[(3-methyl-2,5-dioxo-2,5-dihydro-1H-pyrrol-1yl)amino]pyrimidin-4-yl}benzenesulphonamide

Guidance literature:: Multi-step reaction with 2 steps

1: hydrazine / tetrahydrofuran / 6 h / 70 °C / Heating / reflux

2: methanol; chloroform / 4 h / 80 °C / Heating / reflux

With hydrazine; In tetrahydrofuran; methanol; chloroform;