2-{4-[2-(5,6-dihydro-[1,3]dithiolo[4,5-b][1,4]dithiin-2-ylidene)-5-methylsulfanyl-[1,3]dithiol-4-yl]-phenyl}-4,4,5,5-tetramethyl-imidazolidine-1,3-diol

Base Information

Chemical Name:2-{4-[2-(5,6-dihydro-[1,3]dithiolo[4,5-b][1,4]dithiin-2-ylidene)-5-methylsulfanyl-[1,3]dithiol-4-yl]-phenyl}-4,4,5,5-tetramethyl-imidazolidine-1,3-diol
CAS No.:241156-91-2
Molecular Formula:C₂₂H₂₆N₂O₂S₇
Molecular Weight:574.923
Hs Code.:

2-{4-[2-(5,6-dihydro-[1,3]dithiolo[4,5-<i>b</i>][1,4]dithiin-2-ylidene)-5-methylsulfanyl-[1,3]dithiol-4-yl]-phenyl}-4,4,5,5-tetramethyl-imidazolidine-1,3-diol

Synonyms:2-{4-[2-(5,6-dihydro-[1,3]dithiolo[4,5-b][1,4]dithiin-2-ylidene)-5-methylsulfanyl-[1,3]dithiol-4-yl]-phenyl}-4,4,5,5-tetramethyl-imidazolidine-1,3-diol

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Chemical Property of 2-{4-[2-(5,6-dihydro-[1,3]dithiolo[4,5-b][1,4]dithiin-2-ylidene)-5-methylsulfanyl-[1,3]dithiol-4-yl]-phenyl}-4,4,5,5-tetramethyl-imidazolidine-1,3-diol

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Technology Process of 2-{4-[2-(5,6-dihydro-[1,3]dithiolo[4,5-b][1,4]dithiin-2-ylidene)-5-methylsulfanyl-[1,3]dithiol-4-yl]-phenyl}-4,4,5,5-tetramethyl-imidazolidine-1,3-diol

There total 3 articles about 2-{4-[2-(5,6-dihydro-[1,3]dithiolo[4,5-b][1,4]dithiin-2-ylidene)-5-methylsulfanyl-[1,3]dithiol-4-yl]-phenyl}-4,4,5,5-tetramethyl-imidazolidine-1,3-diol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

: 14384-45-3
N,N'-dihydroxy-2,3-dimethylbutane-2,3-diamine

: 241156-88-7
4-[2-(5,6-dihydro-[1,3]dithiolo[4,5-b][1,4]dithiin-2-ylidene)-5-methylsulfanyl-[1,3]dithiol-4-yl]-benzaldehyde

: 241156-91-2
2-{4-[2-(5,6-dihydro-[1,3]dithiolo[4,5-b][1,4]dithiin-2-ylidene)-5-methylsulfanyl-[1,3]dithiol-4-yl]-phenyl}-4,4,5,5-tetramethyl-imidazolidine-1,3-diol

Guidance literature:: With sulfuric acid; In hexane; dichloromethane; Heating;
DOI:10.1016/S0040-4039(99)00925-9

Reference yield:

: 15164-44-0
p-(iodophenyl)carboxaldehyde

: 241156-91-2
2-{4-[2-(5,6-dihydro-[1,3]dithiolo[4,5-b][1,4]dithiin-2-ylidene)-5-methylsulfanyl-[1,3]dithiol-4-yl]-phenyl}-4,4,5,5-tetramethyl-imidazolidine-1,3-diol

Guidance literature:: Multi-step reaction with 2 steps

1.1: LDA; Me₃SnCl / tetrahydrofuran / 3 h / -70 °C

1.2: 55 percent / Na₂CO₃ / Pd(PPh₃)4 / toluene; H₂O / 20 h / Heating

2.1: 90 percent / H₂SO₄ / CH₂Cl₂; hexane / Heating

With sulfuric acid; trimethyltin(IV)chloride; lithium diisopropyl amide; In tetrahydrofuran; hexane; dichloromethane; 1.1: Metallation / 1.2: Substitution / 2.1: Cycloaddition;
DOI:10.1016/S0040-4039(99)00925-9

Reference yield:

: 2-(4-methylsulfanyl-[1,3]dithiol-2-ylidene)-5,6-dihydro-[1,3]dithiolo[4,5-b][1,4]dithiine

: 241156-91-2
2-{4-[2-(5,6-dihydro-[1,3]dithiolo[4,5-b][1,4]dithiin-2-ylidene)-5-methylsulfanyl-[1,3]dithiol-4-yl]-phenyl}-4,4,5,5-tetramethyl-imidazolidine-1,3-diol

Guidance literature:: Multi-step reaction with 2 steps

1.1: LDA; Me₃SnCl / tetrahydrofuran / 3 h / -70 °C

1.2: 55 percent / Na₂CO₃ / Pd(PPh₃)4 / toluene; H₂O / 20 h / Heating

2.1: 90 percent / H₂SO₄ / CH₂Cl₂; hexane / Heating

With sulfuric acid; trimethyltin(IV)chloride; lithium diisopropyl amide; In tetrahydrofuran; hexane; dichloromethane; 1.1: Metallation / 1.2: Substitution / 2.1: Cycloaddition;
DOI:10.1016/S0040-4039(99)00925-9