C₄₂H₅₄O₉

Base Information

Chemical Name:C₄₂H₅₄O₉
CAS No.:1449419-40-2
Molecular Formula:C₄₂H₅₄O₉
Molecular Weight:702.885
Hs Code.:

C<sub>42</sub>H<sub>54</sub>O<sub>9</sub>

Synonyms:C₄₂H₅₄O₉

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Chemical Property of C₄₂H₅₄O₉

Chemical Property:

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Technology Process of C₄₂H₅₄O₉

There total 10 articles about C₄₂H₅₄O₉ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1449419-31-1
C₄₈H₆₈O₉Si

: 1449419-40-2
C₄₂H₅₄O₉

Guidance literature:: With pyridine hydrogenfluoride; In tetrahydrofuran; at 4 ℃; for 22h; Cooling;
DOI:10.1016/j.tet.2013.02.008

Reference yield:

: 1449419-34-4
C₄₃H₅₆O₇

: 1449419-40-2
C₄₂H₅₄O₉

Guidance literature:: Multi-step reaction with 3 steps

1: 1H-imidazole / tetrahydrofuran / 4 h / 20 °C

2: sodium periodate; potassium permanganate / tert-butyl alcohol; aq. phosphate buffer / 0.13 h / 20 °C / pH 7.2 / Inert atmosphere

3: pyridine hydrogenfluoride / tetrahydrofuran / 22 h / 4 °C / Cooling

With 1H-imidazole; potassium permanganate; sodium periodate; pyridine hydrogenfluoride; In tetrahydrofuran; aq. phosphate buffer; tert-butyl alcohol;
DOI:10.1016/j.tet.2013.02.008

Reference yield:

: 1449419-19-5
C₁₆H₂₄O₃S₂

: 1449419-40-2
C₄₂H₅₄O₉

Guidance literature:: Multi-step reaction with 10 steps

1.1: triphenylphosphine; di-isopropyl azodicarboxylate / tetrahydrofuran; toluene / 21 h / 0 - 20 °C

2.1: sodium hydroxide / tetrahydrofuran; water; methanol / 12 h / 0 - 20 °C

3.1: sodium hydride / tetrahydrofuran; mineral oil / 0.5 h / 0 °C

3.2: 21.5 h / 0 - 20 °C

4.1: sodium hydrogencarbonate; methyl iodide / acetonitrile; water / 19 h / 20 °C

5.1: sodium dihydrogenphosphate; 2-methyl-but-2-ene; sodium chlorite / tetrahydrofuran; water; tert-butyl alcohol / 0.5 h / 4 °C

6.1: 2,4,6-trichlorobenzoyl chloride; triethylamine / toluene / 3 h / 20 °C

6.2: 1.5 h / 50 °C

7.1: 2,3-dicyano-5,6-dichloro-p-benzoquinone / dichloromethane; water / 1 h / 20 °C

8.1: 1H-imidazole / tetrahydrofuran / 4 h / 20 °C

9.1: sodium periodate; potassium permanganate / tert-butyl alcohol; aq. phosphate buffer / 0.13 h / 20 °C / pH 7.2 / Inert atmosphere

10.1: pyridine hydrogenfluoride / tetrahydrofuran / 22 h / 4 °C / Cooling

With 1H-imidazole; sodium chlorite; potassium permanganate; sodium periodate; sodium dihydrogenphosphate; 2-methyl-but-2-ene; di-isopropyl azodicarboxylate; 2,4,6-trichlorobenzoyl chloride; sodium hydride; sodium hydrogencarbonate; pyridine hydrogenfluoride; triethylamine; triphenylphosphine; 2,3-dicyano-5,6-dichloro-p-benzoquinone; sodium hydroxide; methyl iodide; In tetrahydrofuran; methanol; aq. phosphate buffer; dichloromethane; water; toluene; acetonitrile; mineral oil; tert-butyl alcohol; 1.1: |Mitsunobu Displacement / 6.1: |Yamaguchi Lactonization / 6.2: |Yamaguchi Lactonization;
DOI:10.1016/j.tet.2013.02.008