2-{4-[2-amino-6-({[2-(4-chlorophenyl)-1,3-thiazol-4-yl]methyl}thio)-3,5-dicyanopyridin-4-yl]phenoxy}ethyl β-alanyl-L-valinate hydrochloride

Base Information

Chemical Name:2-{4-[2-amino-6-({[2-(4-chlorophenyl)-1,3-thiazol-4-yl]methyl}thio)-3,5-dicyanopyridin-4-yl]phenoxy}ethyl β-alanyl-L-valinate hydrochloride
CAS No.:1110660-72-4
Molecular Formula:C₃₃H₃₂ClN₇O₄S₂*ClH
Molecular Weight:726.708
Hs Code.:

Synonyms:2-{4-[2-amino-6-({[2-(4-chlorophenyl)-1,3-thiazol-4-yl]methyl}thio)-3,5-dicyanopyridin-4-yl]phenoxy}ethyl β-alanyl-L-valinate hydrochloride

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Chemical Property of 2-{4-[2-amino-6-({[2-(4-chlorophenyl)-1,3-thiazol-4-yl]methyl}thio)-3,5-dicyanopyridin-4-yl]phenoxy}ethyl β-alanyl-L-valinate hydrochloride

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Technology Process of 2-{4-[2-amino-6-({[2-(4-chlorophenyl)-1,3-thiazol-4-yl]methyl}thio)-3,5-dicyanopyridin-4-yl]phenoxy}ethyl β-alanyl-L-valinate hydrochloride

There total 6 articles about 2-{4-[2-amino-6-({[2-(4-chlorophenyl)-1,3-thiazol-4-yl]methyl}thio)-3,5-dicyanopyridin-4-yl]phenoxy}ethyl β-alanyl-L-valinate hydrochloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: C₃₈H₄₀ClN₇O₆S₂

: 1110660-72-4
2-{4-[2-amino-6-({[2-(4-chlorophenyl)-1,3-thiazol-4-yl]methyl}thio)-3,5-dicyanopyridin-4-yl]phenoxy}ethyl β-alanyl-L-valinate hydrochloride

Guidance literature:: With hydrogenchloride; In dichloromethane; at 20 ℃; for 3h;

Reference yield:

: 32703-87-0
N-tertiarybutoxycarbonyl-β-alanine N-hydroxysuccinimide ester

: 1110660-30-4
2-{4-[2-amino-6-({[2-(4-chlorophenyl)-1,3-thiazol-4-yl]methyl}thio)-3,5-dicyanopyridin-4-yl]phenoxy}ethyl L-valinate trifluoroacetate

: 1110660-72-4
2-{4-[2-amino-6-({[2-(4-chlorophenyl)-1,3-thiazol-4-yl]methyl}thio)-3,5-dicyanopyridin-4-yl]phenoxy}ethyl β-alanyl-L-valinate hydrochloride

Guidance literature:: With hydrogenchloride; N-ethyl-N,N-diisopropylamine; In diethyl ether; dichloromethane; N,N-dimethyl-formamide;

Reference yield:

: 544417-40-5
Capadenoson

: 1110660-72-4
2-{4-[2-amino-6-({[2-(4-chlorophenyl)-1,3-thiazol-4-yl]methyl}thio)-3,5-dicyanopyridin-4-yl]phenoxy}ethyl β-alanyl-L-valinate hydrochloride

Guidance literature:: Multi-step reaction with 4 steps

1: 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; dmap / dichloromethane; N,N-dimethyl-formamide / 20 °C

2: dichloromethane / 2 h / 20 °C

3: N-ethyl-N,N-diisopropylamine / N,N-dimethyl-formamide / 20 °C

4: hydrogenchloride / dichloromethane / 3 h / 20 °C

With hydrogenchloride; dmap; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; N-ethyl-N,N-diisopropylamine; In dichloromethane; N,N-dimethyl-formamide;