Technology Process of C33H32O5
There total 6 articles about C33H32O5 which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
Multi-step reaction with 4 steps
1.1: diisobutylaluminium hydride / toluene / 2 h / -78 °C
2.1: trimethylsilyl trifluoromethanesulfonate / dichloromethane / 0.08 h / -78 °C
2.2: 1 h / 20 °C
3.1: tin(IV) chloride / dichloromethane / 0.08 h / -90 °C
3.2: 1.5 h / 20 °C
4.1: Burgess Reagent / tetrahydrofuran / 1.5 h / 50 °C
With
Burgess Reagent; trimethylsilyl trifluoromethanesulfonate; tin(IV) chloride; diisobutylaluminium hydride;
In
tetrahydrofuran; dichloromethane; toluene;
DOI:10.1016/j.tetlet.2010.12.061
- Guidance literature:
-
Multi-step reaction with 3 steps
1.1: trimethylsilyl trifluoromethanesulfonate / dichloromethane / 0.08 h / -78 °C
1.2: 1 h / 20 °C
2.1: tin(IV) chloride / dichloromethane / 0.08 h / -90 °C
2.2: 1.5 h / 20 °C
3.1: Burgess Reagent / tetrahydrofuran / 1.5 h / 50 °C
With
Burgess Reagent; trimethylsilyl trifluoromethanesulfonate; tin(IV) chloride;
In
tetrahydrofuran; dichloromethane;
DOI:10.1016/j.tetlet.2010.12.061