N-hydroxy-2-oxo-3a-<3,4-(methylenedioxy)phenyl>-2,3,3a,4,5,7a-hexahydroindole

Base Information

Chemical Name:N-hydroxy-2-oxo-3a-<3,4-(methylenedioxy)phenyl>-2,3,3a,4,5,7a-hexahydroindole
CAS No.:82201-76-1
Molecular Formula:C₁₅H₁₅NO₄
Molecular Weight:273.288
Hs Code.:

Synonyms:N-hydroxy-2-oxo-3a-<3,4-(methylenedioxy)phenyl>-2,3,3a,4,5,7a-hexahydroindole

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Chemical Property of N-hydroxy-2-oxo-3a-<3,4-(methylenedioxy)phenyl>-2,3,3a,4,5,7a-hexahydroindole

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Technology Process of N-hydroxy-2-oxo-3a-<3,4-(methylenedioxy)phenyl>-2,3,3a,4,5,7a-hexahydroindole

There total 1 articles about N-hydroxy-2-oxo-3a-<3,4-(methylenedioxy)phenyl>-2,3,3a,4,5,7a-hexahydroindole which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

: 77545-65-4
12-<<1-<3,4-(methylenedioxy)phenyl>cyclohex-2-enyl>acetyl>-9,10-dihydro-9,10-dimethyl-10,9-(epoxymino)anthracene

: 781-43-1
9,10-dimethylanthracene

: 82201-76-1
N-hydroxy-2-oxo-3a-<3,4-(methylenedioxy)phenyl>-2,3,3a,4,5,7a-hexahydroindole

Guidance literature:: In toluene; for 0.25h; Heating;
DOI:10.1021/ja00401a039

Reference yield:

: 82201-76-1
N-hydroxy-2-oxo-3a-<3,4-(methylenedioxy)phenyl>-2,3,3a,4,5,7a-hexahydroindole

: 510-70-3,4517-24-2,22672-76-0
(+/-)-crinane

Guidance literature:: Multi-step reaction with 4 steps

1: pyridine / 0.03 h

2: 1.) H₂, 2.) TiCl₃ / Pd/C / 1.) EtOAc, 2.) MeOH, H₂O

3: 91 percent / LiAlH₄ / tetrahydrofuran / 3 h / Heating

4: 90 percent / tetrahydrofuran / 30 h / 40 °C

With pyridine; lithium aluminium tetrahydride; titanium(III) chloride; hydrogen; palladium on activated charcoal; In tetrahydrofuran;
DOI:10.1021/ja00401a039