4-(4,5-dihydro-1-phenyl-5-thioxo-1,3,4-triazol-2-yl)-3-methyl-1-phenyl-Δ²-pyrazolin-5-one

Base Information

• Chemical Name: 4-(4,5-dihydro-1-phenyl-5-thioxo-1,3,4-triazol-2-yl)-3-methyl-1-phenyl-Δ²-pyrazolin-5-one
• CAS No.: 433292-90-1
• Molecular Formula: C₁₈H₁₅N₅OS
• Molecular Weight: 349.416

Synonyms:4-(4,5-dihydro-1-phenyl-5-thioxo-1,3,4-triazol-2-yl)-3-methyl-1-phenyl-Δ²-pyrazolin-5-one

Chemical Property of 4-(4,5-dihydro-1-phenyl-5-thioxo-1,3,4-triazol-2-yl)-3-methyl-1-phenyl-Δ²-pyrazolin-5-one

Chemical Property:

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Technology Process of 4-(4,5-dihydro-1-phenyl-5-thioxo-1,3,4-triazol-2-yl)-3-methyl-1-phenyl-Δ²-pyrazolin-5-one

There total 3 articles about 4-(4,5-dihydro-1-phenyl-5-thioxo-1,3,4-triazol-2-yl)-3-methyl-1-phenyl-Δ²-pyrazolin-5-one which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 66.0%

N1-(4,5-dihydro-3-methyl-5-oxo-1-phenylpyrazol-4-yl)thiocarbonyl-N4-phenylthiosemicarbazide (433292-89-8) → 4-(4,5-dihydro-1-phenyl-5-thioxo-1,3,4-triazol-2-yl)-3-methyl-1-phenyl-Δ2-pyrazolin-5-one (433292-90-1)

Guidance literature:

With sodium hydroxide; for 1h;

Reference yield:

phenyl isothiocyanate (103-72-0) → 4-(4,5-dihydro-1-phenyl-5-thioxo-1,3,4-triazol-2-yl)-3-methyl-1-phenyl-Δ2-pyrazolin-5-one (433292-90-1)

Guidance literature:

Multi-step reaction with 2 steps

1: 79 percent / ethanol / 1 h / Heating

2: 66 percent / aq, NaOH / 1 h

With sodium hydroxide; In ethanol;

Reference yield:

3-methyl-5-oxo-1-phenyl-Δ2-pyrazoline-4-thiocarbohydrazide (57624-77-8) → 4-(4,5-dihydro-1-phenyl-5-thioxo-1,3,4-triazol-2-yl)-3-methyl-1-phenyl-Δ2-pyrazolin-5-one (433292-90-1)

Guidance literature:

Multi-step reaction with 2 steps

1: 79 percent / ethanol / 1 h / Heating

2: 66 percent / aq, NaOH / 1 h

With sodium hydroxide; In ethanol;

upstream raw materials:

N¹-(4,5-dihydro-3-methyl-5-oxo-1-phenylpyrazol-4-yl)thiocarbonyl-N⁴-phenylthiosemicarbazide

phenyl isothiocyanate

3-methyl-5-oxo-1-phenyl-Δ²-pyrazoline-4-thiocarbohydrazide

Downstream raw materials:

2-[5-chloro-1-phenyl-4-(4-phenyl-5-thioxo-4,5-dihydro-1H-[1,2,4]triazol-3-yl)-1H-pyrazol-3-yl]-3-dimethylamino-propenal

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