1,6-dihydro-6-oxo-2-phenyl-1-(phenylmethyl)-5-pyrimidinecarboxylic acid

Base Information

Chemical Name:1,6-dihydro-6-oxo-2-phenyl-1-(phenylmethyl)-5-pyrimidinecarboxylic acid
CAS No.:1270000-73-1
Molecular Formula:C₁₈H₁₄N₂O₃
Molecular Weight:306.321
Hs Code.:

Synonyms:1,6-dihydro-6-oxo-2-phenyl-1-(phenylmethyl)-5-pyrimidinecarboxylic acid

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Chemical Property of 1,6-dihydro-6-oxo-2-phenyl-1-(phenylmethyl)-5-pyrimidinecarboxylic acid

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Technology Process of 1,6-dihydro-6-oxo-2-phenyl-1-(phenylmethyl)-5-pyrimidinecarboxylic acid

There total 4 articles about 1,6-dihydro-6-oxo-2-phenyl-1-(phenylmethyl)-5-pyrimidinecarboxylic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1270000-95-7
ethyl 1,6-dihydro-6-oxo-2-phenyl-1-(phenylmethyl)-5-pyrimidinecarboxylate

: 1270000-73-1
1,6-dihydro-6-oxo-2-phenyl-1-(phenylmethyl)-5-pyrimidinecarboxylic acid

Guidance literature:: ethyl 1,6-dihydro-6-oxo-2-phenyl-1-(phenylmethyl)-5-pyrimidinecarboxylate; With lithium iodide; In pyridine; at 20 ℃; for 76h; Reflux;

With hydrogenchloride; In water; pH=1;

Reference yield:

: 15421-92-8
N-benzylbenzamidine

: 1270000-73-1
1,6-dihydro-6-oxo-2-phenyl-1-(phenylmethyl)-5-pyrimidinecarboxylic acid

Guidance literature:: Multi-step reaction with 2 steps

1.1: ethanol / 24 h / Reflux

2.1: pyridine; lithium iodide / 76 h / 20 °C / Reflux

2.2: pH 7

With pyridine; lithium iodide; In ethanol;

Reference yield:

: 100-46-9
benzylamine

: 1270000-73-1
1,6-dihydro-6-oxo-2-phenyl-1-(phenylmethyl)-5-pyrimidinecarboxylic acid

Guidance literature:: Multi-step reaction with 3 steps

1.1: triethylamine / N,N-dimethyl-formamide / 1 h / 20 °C

1.2: 24 h / 65 °C

2.1: ethanol / 24 h / Reflux

3.1: pyridine; lithium iodide / 76 h / 20 °C / Reflux

3.2: pH 7

With pyridine; triethylamine; lithium iodide; In ethanol; N,N-dimethyl-formamide;