Boc-PheΨGly

Base Information

Chemical Name:Boc-PheΨGly
CAS No.:118387-85-2
Molecular Formula:C₁₇H₂₅NO₄
Molecular Weight:307.39
Hs Code.:

Synonyms:Boc-PheΨGly

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Chemical Property of Boc-PheΨGly

Chemical Property:

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Technology Process of Boc-PheΨGly

There total 8 articles about Boc-PheΨGly which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 82042-48-6
(S)-5-<(tert-Butoxycarbonyl)amino>-6-phenyl-(E)-3-hexenoic acid

: 118387-85-2
Boc-PheΨGly

Guidance literature:: With hydrogen; palladium on activated charcoal; In isopropyl alcohol; at 20 ℃; under 2637.5 Torr;
DOI:10.1021/jm00164a058

Reference yield:

: 72155-45-4
Boc-L-phenylalaninal

: 118387-85-2
Boc-PheΨGly

Guidance literature:: Multi-step reaction with 3 steps

1: 1.) n-BuLi / 1.) THF, hexane, -80 deg C, 1 h, 2.) a) -80 deg C, 1 h, b) room temp.

2: 1.) (cyclohexyl)2BH, 2.) 2 N NaOH, 30percent H₂O₂ / 1.) THF, 0 deg C, 1 h, 2.) MeOH, room temp., 1 h

3: 0.45 g / H₂ / 10percent Pd/C / propan-2-ol / 20 °C / 2637.5 Torr

With sodium hydroxide; n-butyllithium; bis(cyclohexanyl)borane; hydrogen; dihydrogen peroxide; palladium on activated charcoal; In isopropyl alcohol;
DOI:10.1021/jm00164a058

Reference yield:

: 82001-64-7
(E)-(S)-<1-(phenylmethyl)-5-(trimethylsilyl)-3-hexen-5-ynyl>carbamic acid 1,1-dimethylethyl ester

: 118387-85-2
Boc-PheΨGly

Guidance literature:: Multi-step reaction with 2 steps

1: 1.) (cyclohexyl)2BH, 2.) 2 N NaOH, 30percent H₂O₂ / 1.) THF, 0 deg C, 1 h, 2.) MeOH, room temp., 1 h

2: 0.45 g / H₂ / 10percent Pd/C / propan-2-ol / 20 °C / 2637.5 Torr

With sodium hydroxide; bis(cyclohexanyl)borane; hydrogen; dihydrogen peroxide; palladium on activated charcoal; In isopropyl alcohol;
DOI:10.1021/jm00164a058