[(4-butyl-6-phenylpyridin-2ylmethylene)-(2,6-diisopropylphenyl)amine]NiBr₂

Base Information

Chemical Name:[(4-butyl-6-phenylpyridin-2ylmethylene)-(2,6-diisopropylphenyl)amine]NiBr₂
CAS No.:1403850-09-8
Molecular Formula:C₂₈H₃₄Br₂N₂Ni
Molecular Weight:617.089
Hs Code.:

[(4-butyl-6-phenylpyridin-2ylmethylene)-(2,6-diisopropylphenyl)amine]NiBr<sub>2</sub>

Synonyms:[(4-butyl-6-phenylpyridin-2ylmethylene)-(2,6-diisopropylphenyl)amine]NiBr₂

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Chemical Property of [(4-butyl-6-phenylpyridin-2ylmethylene)-(2,6-diisopropylphenyl)amine]NiBr₂

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Technology Process of [(4-butyl-6-phenylpyridin-2ylmethylene)-(2,6-diisopropylphenyl)amine]NiBr₂

There total 2 articles about [(4-butyl-6-phenylpyridin-2ylmethylene)-(2,6-diisopropylphenyl)amine]NiBr₂ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 57.6%

: 28923-39-9
nickel(II) bromide dimethoxyethane

: 24544-04-5
2,6-diisopropylbenzenamine

: 1403850-03-2
4-butyl-6-phenylpyridin-2-carbaldehyde

: 1403850-09-8
[(4-butyl-6-phenylpyridin-2ylmethylene)-(2,6-diisopropylphenyl)amine]NiBr₂

Guidance literature:: With acetic acid; for 4h; Reflux; Inert atmosphere; Schlenk technique;
DOI:10.1016/j.jorganchem.2012.08.005

Reference yield:

: 1008-89-5
2-phenylpyridine

: 1403850-09-8
[(4-butyl-6-phenylpyridin-2ylmethylene)-(2,6-diisopropylphenyl)amine]NiBr₂

Guidance literature:: Multi-step reaction with 2 steps

1.1: 2-(N,N-dimethylamino)ethanol / hexane / 0.5 h / Inert atmosphere; Schlenk technique

1.2: 0.5 h / 0 °C / Inert atmosphere; Schlenk technique

1.3: 1 h / -78 °C / Inert atmosphere; Schlenk technique

2.1: acetic acid / 4 h / Reflux; Inert atmosphere; Schlenk technique

With 2-(N,N-dimethylamino)ethanol; acetic acid; In hexane;
DOI:10.1016/j.jorganchem.2012.08.005