5'-S-acetyl-2',3'-O-isopropylidene-6-{[(4-methoxyphenyl)diphenylmethoxy]methyl}uridine

Base Information

• Chemical Name: 5'-S-acetyl-2',3'-O-isopropylidene-6-{[(4-methoxyphenyl)diphenylmethoxy]methyl}uridine
• CAS No.: 1040238-93-4
• Molecular Formula: C₃₅H₃₆N₂O₈S
• Molecular Weight: 644.745

Synonyms:5'-S-acetyl-2',3'-O-isopropylidene-6-{[(4-methoxyphenyl)diphenylmethoxy]methyl}uridine

Chemical Property of 5'-S-acetyl-2',3'-O-isopropylidene-6-{[(4-methoxyphenyl)diphenylmethoxy]methyl}uridine

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Technology Process of 5'-S-acetyl-2',3'-O-isopropylidene-6-{[(4-methoxyphenyl)diphenylmethoxy]methyl}uridine

There total 1 articles about 5'-S-acetyl-2',3'-O-isopropylidene-6-{[(4-methoxyphenyl)diphenylmethoxy]methyl}uridine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

2',3'-O-isopropylidene-6-{[(4-methoxyphenyl)(diphenyl)methoxy]methyl}-5'-O-[(4-methylphenyl)sulfonyl]uridine + potassium thioacetate (10387-40-3) → 5'-S-acetyl-2',3'-O-isopropylidene-6-{[(4-methoxyphenyl)diphenylmethoxy]methyl}uridine (1040238-93-4)

Guidance literature:

In N,N-dimethyl-formamide; at 40 - 75 ℃; for 3h;

DOI:10.1002/hlca.200890071

Reference yield: 75.0%

N(6)-benzoyl-8-(bromomethyl)-5'-O-[dimethyl(1,1,2-trimethylpropyl)silyl]-2',3'-O-isopropylideneadenosine (1040239-08-4) + 5'-S-acetyl-2',3'-O-isopropylidene-6-{[(4-methoxyphenyl)diphenylmethoxy]methyl}uridine (1040238-93-4) → 5'-O-[dimethyl(1,1,2-trimethylpropyl)silyl]-2',3'-O-isopropylideneadenosine-8-methyl-(8'->5'-S)-2',3'-O-isopropylidene-6-{[(4-methoxyphenyl)diphenylmethoxy]methyl}-5'-thiouridine (1040239-45-9)

Guidance literature:

With sodium methylate; In methanol; at 23 ℃; for 14h;

DOI:10.1002/hlca.200890071

Reference yield:

5'-S-acetyl-2',3'-O-isopropylidene-6-{[(4-methoxyphenyl)diphenylmethoxy]methyl}uridine (1040238-93-4) → C33H34N2O7S

Guidance literature:

With methanol; potassium carbonate; at 23 ℃; for 0.166667h; Inert atmosphere;

DOI:10.1002/hlca.200900203

upstream raw materials:

potassium thioacetate

Downstream raw materials:

5'-O-[dimethyl(1,1,2-trimethylpropyl)silyl]-2',3'-O-isopropylideneadenosine-8-methyl-(8'->5'-S)-2',3'-O-isopropylidene-6-{[(4-methoxyphenyl)diphenylmethoxy]methyl}-5'-thiouridine

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