N¹,N³-Bis-[1-(4-chloro-phenyl)-meth-(E)-ylidene]-4-methyl-benzene-1,3-diamine

Base Information

• Chemical Name: N¹,N³-Bis-[1-(4-chloro-phenyl)-meth-(E)-ylidene]-4-methyl-benzene-1,3-diamine
• CAS No.: 134667-96-2
• Molecular Formula: C₂₁H₁₆Cl₂N₂
• Molecular Weight: 367.277

Synonyms:N¹,N³-Bis-[1-(4-chloro-phenyl)-meth-(E)-ylidene]-4-methyl-benzene-1,3-diamine

Chemical Property of N¹,N³-Bis-[1-(4-chloro-phenyl)-meth-(E)-ylidene]-4-methyl-benzene-1,3-diamine

Chemical Property:

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Technology Process of N¹,N³-Bis-[1-(4-chloro-phenyl)-meth-(E)-ylidene]-4-methyl-benzene-1,3-diamine

There total 1 articles about N¹,N³-Bis-[1-(4-chloro-phenyl)-meth-(E)-ylidene]-4-methyl-benzene-1,3-diamine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

4-methylbenzene-1,3-diamine (95-80-7,71111-07-4) + 4-chlorobenzaldehyde (104-88-1) → N1,N3-Bis-[1-(4-chloro-phenyl)-meth-(E)-ylidene]-4-methyl-benzene-1,3-diamine (134667-96-2)

Guidance literature:

In ethanol; for 5h; Heating; also ZnCl₂, 160 deg C, 0.5 h, 180 deg C, 5 min;

Reference yield: 76.0%

2,4-Dichlorophenoxyacetic acid (94-75-7,89300-30-1) + N1,N3-Bis-[1-(4-chloro-phenyl)-meth-(E)-ylidene]-4-methyl-benzene-1,3-diamine (134667-96-2) → 3-(2,4-dichlorophenoxy)-1-(3-(3-(2,4-dichlorophenoxy)-2-oxo-4-(4-chlorophenyl)azetidin-1-yl)-4-methylphenyl)-4-(4-chlorophenyl)azetidin-2-one

Guidance literature:

With Vilsmeier reagent; triethylamine; In dichloromethane; at -5 - 20 ℃;

DOI:10.1002/jhet.455

Reference yield: 66.0%

N1,N3-Bis-[1-(4-chloro-phenyl)-meth-(E)-ylidene]-4-methyl-benzene-1,3-diamine (134667-96-2) + 2-mercaptopropanoic acid (79-42-5) → C27H24Cl2N2O2S2 (134667-83-7)

Guidance literature:

In benzene; for 6h; Heating;

upstream raw materials:

4-methylbenzene-1,3-diamine

4-chlorobenzaldehyde

Downstream raw materials:

C₂₅H₂₀Cl₂N₂O₂S₂

C₂₇H₂₄Cl₂N₂O₂S₂

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