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Technology Process of C82H58S2

C82H58S2

Base Information
  • Chemical Name:C82H58S2
  • CAS No.:1001208-65-6
  • Molecular Formula:C82H58S2
  • Molecular Weight:1107.49
  • Hs Code.:
C<sub>82</sub>H<sub>58</sub>S<sub>2</sub>

Synonyms:C82H58S2

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Chemical Property of C82H58S2
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Technology Process of C82H58S2

There total 1 articles about C82H58S2 which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 83.0%

3,3'''',5,5''''-tetrakis(bromomethyl)-3',3''',4',4''',5',5''',6',6'''-octaphenyl-1,1':2',1'':4'',1''':2''',1''''-o,p,o-quinquephenyl
1001208-64-5

3,3'''',5,5''''-tetrakis(bromomethyl)-3',3''',4',4''',5',5''',6',6'''-octaphenyl-1,1':2',1'':4'',1''':2''',1''''-o,p,o-quinquephenyl

C<sub>82</sub>H<sub>58</sub>S<sub>2</sub>
1001208-65-6

C82H58S2

Guidance literature:
With sodium sulfide; aluminum oxide; In ethanol; dichloromethane; at 20 ℃; for 12h;
DOI:10.1021/ol702703b

Reference yield: 19.0%

C<sub>82</sub>H<sub>58</sub>S<sub>2</sub>
1001208-65-6

C82H58S2

C<sub>82</sub>H<sub>54</sub>
1001208-66-7

C82H54

Guidance literature:
Multistep reaction.;
DOI:10.1021/ol702703b

Reference yield:

C<sub>82</sub>H<sub>58</sub>S<sub>2</sub>
1001208-65-6

C82H58S2

dimethoxymethylium tetrafluoroborate
18346-68-4,60218-70-4,139200-70-7

dimethoxymethylium tetrafluoroborate

C<sub>84</sub>H<sub>62</sub>S<sub>2</sub>

C84H62S2

C<sub>84</sub>H<sub>62</sub>S<sub>2</sub>

C84H62S2

Guidance literature:
C82H58S2; dimethoxymethylium tetrafluoroborate; In dichloromethane; at 20 ℃; for 1h;
With potassium tert-butylate; In tetrahydrofuran; at 20 ℃; Further stages. Title compound not separated from byproducts.;
DOI:10.1021/ol702703b
upstream raw materials:

3,3'''',5,5''''-tetrakis(bromomethyl)-3',3''',4',4''',5',5''',6',6'''-octaphenyl-1,1':2',1'':4'',1''':2''',1''''-o,p,o-quinquephenyl

Downstream raw materials:

C82H54

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