iron(II) tetraphenylporphyrin (thiophenyl)chlorocarbene

Base Information

Chemical Name:iron(II) tetraphenylporphyrin (thiophenyl)chlorocarbene
CAS No.:80719-01-3
Molecular Formula:C₅₁H₃₃ClFeN₄S*H₂O
Molecular Weight:843.231
Hs Code.:

Synonyms:iron(II) tetraphenylporphyrin (thiophenyl)chlorocarbene

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Chemical Property of iron(II) tetraphenylporphyrin (thiophenyl)chlorocarbene

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Technology Process of iron(II) tetraphenylporphyrin (thiophenyl)chlorocarbene

There total 1 articles about iron(II) tetraphenylporphyrin (thiophenyl)chlorocarbene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.0%

: 16456-81-8,170645-84-8
meso-tetraphenylporphyrin iron(III) chloride

: 701-65-5
(trichloromethylthio)benzene

: 80719-01-3
iron(II) tetraphenylporphyrin (thiophenyl)chlorocarbene

Guidance literature:: With iron; In dichloromethane; N,N-dimethyl-formamide; Fe powder adding to a soln. of Fe(III) complex in CH2Cl2-DMF, vigorously stirring for 15 min under Ar, ligand soln. in CH2Cl2 adding, stirring for 2 h, filtering, evapg.; purified by recrystn. from minimum CH2Cl2 and excess of MeOH; identified by elem. anal., UV, IR, mass and NMR spectra;
DOI:10.1021/ic00135a066