(-)-<(6S,7S,10S)-6,10-Epoxy-5,6,7,8,9,10-hexahydro-2,3-dimethoxy-10-methylbenzocycloocten-7-yl>-4-methylbenzolsulfonat

Base Information

Chemical Name:(-)-<(6S,7S,10S)-6,10-Epoxy-5,6,7,8,9,10-hexahydro-2,3-dimethoxy-10-methylbenzocycloocten-7-yl>-4-methylbenzolsulfonat
CAS No.:153994-10-6
Molecular Formula:C₂₂H₂₆O₆S
Molecular Weight:418.511
Hs Code.:

Synonyms:(-)-<(6S,7S,10S)-6,10-Epoxy-5,6,7,8,9,10-hexahydro-2,3-dimethoxy-10-methylbenzocycloocten-7-yl>-4-methylbenzolsulfonat

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Chemical Property of (-)-<(6S,7S,10S)-6,10-Epoxy-5,6,7,8,9,10-hexahydro-2,3-dimethoxy-10-methylbenzocycloocten-7-yl>-4-methylbenzolsulfonat

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Technology Process of (-)-<(6S,7S,10S)-6,10-Epoxy-5,6,7,8,9,10-hexahydro-2,3-dimethoxy-10-methylbenzocycloocten-7-yl>-4-methylbenzolsulfonat

There total 2 articles about (-)-<(6S,7S,10S)-6,10-Epoxy-5,6,7,8,9,10-hexahydro-2,3-dimethoxy-10-methylbenzocycloocten-7-yl>-4-methylbenzolsulfonat which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 84.0%

: 98-59-9
p-toluenesulfonyl chloride

: 153994-09-3
(6S,7S,10S)-(-)-6,10-Epoxy-5,6,7,8,9,10-hexahydro-2,3-dimethoxy-10-methylbenzocycloocten-7-ol

: 153994-10-6
(-)-<(6S,7S,10S)-6,10-Epoxy-5,6,7,8,9,10-hexahydro-2,3-dimethoxy-10-methylbenzocycloocten-7-yl>-4-methylbenzolsulfonat

Guidance literature:: In pyridine; at 70 ℃; for 5h;
DOI:10.1002/ardp.19933261011

Reference yield:

: 145653-75-4
(6S,10S)-(-)-6,10-Epoxy-5,8,9,10-tetrahydro-2,3-dimethoxy-10-methylbenzocycloocten-7(6H)-on

: 153994-10-6
(-)-<(6S,7S,10S)-6,10-Epoxy-5,6,7,8,9,10-hexahydro-2,3-dimethoxy-10-methylbenzocycloocten-7-yl>-4-methylbenzolsulfonat

Guidance literature:: Multi-step reaction with 2 steps

1: 73 percent / NaBH₄ / ethanol / 54 h / Ambient temperature

2: 84 percent / pyridine / 5 h / 70 °C

With sodium tetrahydroborate; In pyridine; ethanol;
DOI:10.1002/ardp.19933261011