N-(2S,3R,4S,5S)-2,3,4,5,6-pentaacetoxyhexyl-1-yl-N-methyl-N'-phenylthiourea

Base Information

Chemical Name:N-(2S,3R,4S,5S)-2,3,4,5,6-pentaacetoxyhexyl-1-yl-N-methyl-N'-phenylthiourea
CAS No.:266363-17-1
Molecular Formula:C₂₄H₃₂N₂O₁₀S
Molecular Weight:540.591
Hs Code.:

Synonyms:N-(2S,3R,4S,5S)-2,3,4,5,6-pentaacetoxyhexyl-1-yl-N-methyl-N'-phenylthiourea

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Chemical Property of N-(2S,3R,4S,5S)-2,3,4,5,6-pentaacetoxyhexyl-1-yl-N-methyl-N'-phenylthiourea

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Technology Process of N-(2S,3R,4S,5S)-2,3,4,5,6-pentaacetoxyhexyl-1-yl-N-methyl-N'-phenylthiourea

There total 1 articles about N-(2S,3R,4S,5S)-2,3,4,5,6-pentaacetoxyhexyl-1-yl-N-methyl-N'-phenylthiourea which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 65.0%

: 108-24-7
acetic anhydride

: 266363-14-8
N-(2S,3R,4S,5S)-2,3,4,5,6-pentahydroxyhexyl-1-yl-N-methyl-N'-phenylthiourea

: 266363-17-1
N-(2S,3R,4S,5S)-2,3,4,5,6-pentaacetoxyhexyl-1-yl-N-methyl-N'-phenylthiourea

Guidance literature:: With sodium acetate; at 20 ℃; for 168h;
DOI:10.1016/S0040-4020(00)00022-3

Reference yield:

: 266363-17-1
N-(2S,3R,4S,5S)-2,3,4,5,6-pentaacetoxyhexyl-1-yl-N-methyl-N'-phenylthiourea

: 6-[N-methyl-N-(2S,3R,4S,5S)-2',3',4',5',6'-pentaacetoxyhexyl-1-yl]amino-4,5-dimethoxycarbonyl-1,3-diphenylpyridin-2-one

Guidance literature:: Multi-step reaction with 2 steps

1: Et₃N / CHCl₃ / 3 h / Heating

2: 0.85 g / CHCl₃ / 1 h / 20 °C

With triethylamine; In chloroform; 1: Condensation / 2: Cycloaddition;
DOI:10.1016/S0040-4020(00)00022-3