2-(3,4-dichlorobenzylamino)-9-(4-methoxybutyl)-8-methyl-6-oxo-3-deazapurine

Base Information

Chemical Name:2-(3,4-dichlorobenzylamino)-9-(4-methoxybutyl)-8-methyl-6-oxo-3-deazapurine
CAS No.:1319732-04-1
Molecular Formula:C₁₉H₂₂Cl₂N₄O₂
Molecular Weight:409.315
Hs Code.:

Synonyms:2-(3,4-dichlorobenzylamino)-9-(4-methoxybutyl)-8-methyl-6-oxo-3-deazapurine

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Chemical Property of 2-(3,4-dichlorobenzylamino)-9-(4-methoxybutyl)-8-methyl-6-oxo-3-deazapurine

Chemical Property:

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Technology Process of 2-(3,4-dichlorobenzylamino)-9-(4-methoxybutyl)-8-methyl-6-oxo-3-deazapurine

There total 4 articles about 2-(3,4-dichlorobenzylamino)-9-(4-methoxybutyl)-8-methyl-6-oxo-3-deazapurine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 75.0%

: 1319732-03-0
9-(4-methoxybutyl)-2-chloro-6-benzyloxy-8-methylimidazo[4,5-c]pyridine

: 102-49-8
3,4-dichlorobenzyl amine

: 1319732-04-1
2-(3,4-dichlorobenzylamino)-9-(4-methoxybutyl)-8-methyl-6-oxo-3-deazapurine

Guidance literature:: at 155 ℃; for 24h; Inert atmosphere;
DOI:10.1016/j.bmcl.2011.05.093

Reference yield:

: 3,4-diamino-2,6-dichloropyridine dihydrochloride

: 1319732-04-1
2-(3,4-dichlorobenzylamino)-9-(4-methoxybutyl)-8-methyl-6-oxo-3-deazapurine

Guidance literature:: Multi-step reaction with 4 steps

1.1: phosphoric acid / 16 h / 80 °C

2.1: sodium / 120 °C

3.1: tetra-(n-butyl)ammonium iodide; potassium carbonate / N,N-dimethyl-formamide / 20 °C

3.2: 16 h / 45 °C

4.1: 24 h / 155 °C / Inert atmosphere

With phosphoric acid; sodium; tetra-(n-butyl)ammonium iodide; potassium carbonate; In N,N-dimethyl-formamide;
DOI:10.1016/j.bmcl.2011.05.093

Reference yield:

: 579486-60-5
4,6-dichloro-2-methyl-1H-imidazo[4,5-c]pyridine

: 1319732-04-1
2-(3,4-dichlorobenzylamino)-9-(4-methoxybutyl)-8-methyl-6-oxo-3-deazapurine

Guidance literature:: Multi-step reaction with 3 steps

1.1: sodium / 120 °C

2.1: tetra-(n-butyl)ammonium iodide; potassium carbonate / N,N-dimethyl-formamide / 20 °C

2.2: 16 h / 45 °C

3.1: 24 h / 155 °C / Inert atmosphere

With sodium; tetra-(n-butyl)ammonium iodide; potassium carbonate; In N,N-dimethyl-formamide;
DOI:10.1016/j.bmcl.2011.05.093