methyl (11S)-11-[[(2-O-acetyl-3,4-di-O-benzyl-β-D-quinovosyl)-(1->2)-(3,4,6-tri-O-benzyl-β-D-glucopyranosyl)-(1->2)-3,4-O-isopropylidene-β-D-fucopyranosyl]oxy]hexadecanoate

Base Information

Chemical Name:methyl (11S)-11-[[(2-O-acetyl-3,4-di-O-benzyl-β-D-quinovosyl)-(1->2)-(3,4,6-tri-O-benzyl-β-D-glucopyranosyl)-(1->2)-3,4-O-isopropylidene-β-D-fucopyranosyl]oxy]hexadecanoate
CAS No.:660852-24-4
Molecular Formula:C₇₅H₁₀₀O₁₇
Molecular Weight:1273.61
Hs Code.:

methyl (11S)-11-[[(2-O-acetyl-3,4-di-O-benzyl-β-D-quinovosyl)-(1->2)-(3,4,6-tri-O-benzyl-β-D-glucopyranosyl)-(1->2)-3,4-O-isopropylidene-β-D-fucopyranosyl]oxy]hexadecanoate

Synonyms:methyl (11S)-11-[[(2-O-acetyl-3,4-di-O-benzyl-β-D-quinovosyl)-(1->2)-(3,4,6-tri-O-benzyl-β-D-glucopyranosyl)-(1->2)-3,4-O-isopropylidene-β-D-fucopyranosyl]oxy]hexadecanoate

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Chemical Property of methyl (11S)-11-[[(2-O-acetyl-3,4-di-O-benzyl-β-D-quinovosyl)-(1->2)-(3,4,6-tri-O-benzyl-β-D-glucopyranosyl)-(1->2)-3,4-O-isopropylidene-β-D-fucopyranosyl]oxy]hexadecanoate

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Technology Process of methyl (11S)-11-[[(2-O-acetyl-3,4-di-O-benzyl-β-D-quinovosyl)-(1->2)-(3,4,6-tri-O-benzyl-β-D-glucopyranosyl)-(1->2)-3,4-O-isopropylidene-β-D-fucopyranosyl]oxy]hexadecanoate

There total 3 articles about methyl (11S)-11-[[(2-O-acetyl-3,4-di-O-benzyl-β-D-quinovosyl)-(1->2)-(3,4,6-tri-O-benzyl-β-D-glucopyranosyl)-(1->2)-3,4-O-isopropylidene-β-D-fucopyranosyl]oxy]hexadecanoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 60.0%

: 2-O-acetyl-3,4-di-O-benzyl-α-D-quinovosyl trichloroacetimidate

: 660852-23-3
methyl (11S)-11-[[(3,4,6-tri-O-benzyl-β-D-glucopyranosyl)-(1->2)-3,4-O-isopropylidene-β-D-fucopyranosyl]oxy]hexadecanoate

: 660852-24-4
methyl (11S)-11-[[(2-O-acetyl-3,4-di-O-benzyl-β-D-quinovosyl)-(1->2)-(3,4,6-tri-O-benzyl-β-D-glucopyranosyl)-(1->2)-3,4-O-isopropylidene-β-D-fucopyranosyl]oxy]hexadecanoate

Guidance literature:: With boron trifluoride diethyl etherate; In diethyl ether; dichloromethane; at -20 ℃; for 1h;
DOI:10.1021/jo030244c

Reference yield:

: 180782-63-2
1-(methoxycarbonyl)pentadec-10(S)-yl 3,4-O-isopropylidene-β-D-fucopyranoside

: 660852-24-4
methyl (11S)-11-[[(2-O-acetyl-3,4-di-O-benzyl-β-D-quinovosyl)-(1->2)-(3,4,6-tri-O-benzyl-β-D-glucopyranosyl)-(1->2)-3,4-O-isopropylidene-β-D-fucopyranosyl]oxy]hexadecanoate

Guidance literature:: Multi-step reaction with 3 steps

1: 70 percent / BF₃*OEt₂ / CH₂Cl₂; diethyl ether / 1 h / -20 °C

2: 95 percent / NaOMe / methanol / 4 h / 20 °C

3: 60 percent / BF₃*OEt₂ / CH₂Cl₂; diethyl ether / 1 h / -20 °C

With boron trifluoride diethyl etherate; sodium methylate; In methanol; diethyl ether; dichloromethane;
DOI:10.1021/jo030244c

Reference yield:

: 660852-22-2
methyl (11S)-11-[[(2-O-acetyl-3,4,6-tri-O-benzyl-β-D-glucopyranosyl)-(1->2)-3,4-O-isopropylidene-β-D-fucopyranosyl]oxy]hexadecanoate

: 660852-24-4
methyl (11S)-11-[[(2-O-acetyl-3,4-di-O-benzyl-β-D-quinovosyl)-(1->2)-(3,4,6-tri-O-benzyl-β-D-glucopyranosyl)-(1->2)-3,4-O-isopropylidene-β-D-fucopyranosyl]oxy]hexadecanoate

Guidance literature:: Multi-step reaction with 2 steps

1: 95 percent / NaOMe / methanol / 4 h / 20 °C

2: 60 percent / BF₃*OEt₂ / CH₂Cl₂; diethyl ether / 1 h / -20 °C

With boron trifluoride diethyl etherate; sodium methylate; In methanol; diethyl ether; dichloromethane;
DOI:10.1021/jo030244c