5-benzyloxy-6-[5-(4-fluorobenzyl)furan-2-carbonyl]-4-oxo-4H-pyrane-2-carboxylic acid

Base Information

• Chemical Name: 5-benzyloxy-6-[5-(4-fluorobenzyl)furan-2-carbonyl]-4-oxo-4H-pyrane-2-carboxylic acid
• CAS No.: 500371-62-0
• Molecular Formula: C₂₅H₁₇FO₇
• Molecular Weight: 448.404

Synonyms:5-benzyloxy-6-[5-(4-fluorobenzyl)furan-2-carbonyl]-4-oxo-4H-pyrane-2-carboxylic acid

Chemical Property of 5-benzyloxy-6-[5-(4-fluorobenzyl)furan-2-carbonyl]-4-oxo-4H-pyrane-2-carboxylic acid

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Technology Process of 5-benzyloxy-6-[5-(4-fluorobenzyl)furan-2-carbonyl]-4-oxo-4H-pyrane-2-carboxylic acid

There total 1 articles about 5-benzyloxy-6-[5-(4-fluorobenzyl)furan-2-carbonyl]-4-oxo-4H-pyrane-2-carboxylic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.0%

3-benzyloxy-2-[5-(4-fluorobenzyl)furan-2-carbonyl]-6-hydroxymethylpyrane-4-one (500371-16-4) → 5-benzyloxy-6-[5-(4-fluorobenzyl)furan-2-carbonyl]-4-oxo-4H-pyrane-2-carboxylic acid (500371-62-0)

Guidance literature:

With Jones reagent; In acetone; at 0 - 20 ℃; for 1.5h;

Reference yield: 78.0%

5-benzyloxy-6-[5-(4-fluorobenzyl)furan-2-carbonyl]-4-oxo-4H-pyrane-2-carboxylic acid (500371-62-0) + diazomethyl-trimethyl-silane (18107-18-1) → 5-benzyloxy-6-[5-(4-fluorobenzyl)furan-2-carbonyl]-4-oxo-4H-pyrane-2-carboxylic acid methyl ester (500371-63-1)

Guidance literature:

With acetic acid; In tetrahydrofuran;

Reference yield: 42.0%

5-benzyloxy-6-[5-(4-fluorobenzyl)furan-2-carbonyl]-4-oxo-4H-pyrane-2-carboxylic acid (500371-62-0) + benzylamine (100-46-9) → 5-benzyloxy-6-[5-(4-fluorobenzyl)furan-2-carbonyl]-4-oxo-4H-pyrane-2-carboxylic acid benzylamide (500371-64-2)

Guidance literature:

With benzotriazol-1-ol; N-(3-dimethylaminopropyl)-N-ethylcarbodiimide; In N,N-dimethyl-formamide; at 20 ℃; for 20h;

upstream raw materials:

3-benzyloxy-2-[5-(4-fluorobenzyl)furan-2-carbonyl]-6-hydroxymethylpyrane-4-one

Downstream raw materials:

5-benzyloxy-6-[5-(4-fluorobenzyl)furan-2-carbonyl]-4-oxo-4H-pyrane-2-carboxylic acid benzylamide

5-benzyloxy-6-[5-(4-fluorobenzyl)furan-2-carbonyl]-4-oxo-4H-pyrane-2-carboxylic acid methyl ester

6-[5-(4-fluorobenzyl)furan-2-carbonyl]-5-hydroxy-4-oxo-4H-pyrane-2-carboxylic acid

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