1-(hydroxymethyl)cyclobutyl phenyl selenoxide

Base Information

Chemical Name:1-(hydroxymethyl)cyclobutyl phenyl selenoxide
CAS No.:307494-45-7
Molecular Formula:C₁₁H₁₄O₂Se
Molecular Weight:257.191
Hs Code.:

Synonyms:1-(hydroxymethyl)cyclobutyl phenyl selenoxide

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Chemical Property of 1-(hydroxymethyl)cyclobutyl phenyl selenoxide

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Technology Process of 1-(hydroxymethyl)cyclobutyl phenyl selenoxide

There total 3 articles about 1-(hydroxymethyl)cyclobutyl phenyl selenoxide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 81.0%

: 307494-44-6
1-hydroxymethyl-1-phenylselenocyclobutane

: 307494-45-7
1-(hydroxymethyl)cyclobutyl phenyl selenoxide

Guidance literature:: With sodium periodate; In methanol; water; at 25 ℃; for 0.0833333h;
DOI:10.1021/jm000961o

Reference yield:

: 1666-13-3
diphenyl diselenide

: 307494-45-7
1-(hydroxymethyl)cyclobutyl phenyl selenoxide

Guidance literature:: Multi-step reaction with 3 steps

1.1: NaBH₄ / ethanol / 25 °C

1.2: 94 percent / zinc chloride / CCl₄ / 12 h / 25 °C

2.1: tert-butyllithium / tetrahydrofuran / 6 h / -78 °C

2.2: 41 percent / tetrahydrofuran / 12 h / -78 - 20 °C

3.1: 81 percent / sodium periodate / methanol; H₂O / 0.08 h / 25 °C

With sodium tetrahydroborate; sodium periodate; tert.-butyl lithium; In tetrahydrofuran; methanol; ethanol; water; 1.1: Reduction / 1.2: Condensation / 2.1: Metallation / 2.2: Addition / 3.1: Oxidation;
DOI:10.1021/jm000961o

Reference yield:

: 76373-62-1
1,1-bis(phenylseleno)cyclobutane

: 307494-45-7
1-(hydroxymethyl)cyclobutyl phenyl selenoxide

Guidance literature:: Multi-step reaction with 2 steps

1.1: tert-butyllithium / tetrahydrofuran / 6 h / -78 °C

1.2: 41 percent / tetrahydrofuran / 12 h / -78 - 20 °C

2.1: 81 percent / sodium periodate / methanol; H₂O / 0.08 h / 25 °C

With sodium periodate; tert.-butyl lithium; In tetrahydrofuran; methanol; water; 1.1: Metallation / 1.2: Addition / 2.1: Oxidation;
DOI:10.1021/jm000961o