(3R,4R,5R)-1,3-bis(benzyloxy)-5-((benzyloxy)methyl)-4-((2-naphthylmethyl)oxy)piperidine

Base Information

Chemical Name:(3R,4R,5R)-1,3-bis(benzyloxy)-5-((benzyloxy)methyl)-4-((2-naphthylmethyl)oxy)piperidine
CAS No.:1425377-81-6
Molecular Formula:C₃₈H₃₉NO₄
Molecular Weight:573.732
Hs Code.:

Synonyms:(3R,4R,5R)-1,3-bis(benzyloxy)-5-((benzyloxy)methyl)-4-((2-naphthylmethyl)oxy)piperidine

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Chemical Property of (3R,4R,5R)-1,3-bis(benzyloxy)-5-((benzyloxy)methyl)-4-((2-naphthylmethyl)oxy)piperidine

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Technology Process of (3R,4R,5R)-1,3-bis(benzyloxy)-5-((benzyloxy)methyl)-4-((2-naphthylmethyl)oxy)piperidine

There total 2 articles about (3R,4R,5R)-1,3-bis(benzyloxy)-5-((benzyloxy)methyl)-4-((2-naphthylmethyl)oxy)piperidine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 3,6-di-O-benzyl-4-O-(2-naphthylmethyl)-2-deoxy-D-arabinohexodialdose

: 1425377-81-6
(3R,4R,5R)-1,3-bis(benzyloxy)-5-((benzyloxy)methyl)-4-((2-naphthylmethyl)oxy)piperidine

Guidance literature:: Multi-step reaction with 2 steps

1: methanol; tetrahydrofuran / 2.5 h / 20 °C / Inert atmosphere; Molecular sieve

2: sodium cyanoborohydride; acetic acid / 4.5 h / 20 °C / Inert atmosphere

With sodium cyanoborohydride; acetic acid; In tetrahydrofuran; methanol;
DOI:10.1002/chem.201202374

Reference yield:

: C₄₅H₄₄N₂O₅

: 1425377-81-6
(3R,4R,5R)-1,3-bis(benzyloxy)-5-((benzyloxy)methyl)-4-((2-naphthylmethyl)oxy)piperidine

Guidance literature:: With sodium cyanoborohydride; acetic acid; at 20 ℃; for 4.5h; Inert atmosphere;
DOI:10.1002/chem.201202374

Reference yield: 63.0%

: 1425377-81-6
(3R,4R,5R)-1,3-bis(benzyloxy)-5-((benzyloxy)methyl)-4-((2-naphthylmethyl)oxy)piperidine

: 1353742-35-4
(3R,4R,5R)-1-(benzyloxy)-5-(hydroxymethyl)piperidine-3,4-diol

Guidance literature:: (3R,4R,5R)-1,3-bis(benzyloxy)-5-((benzyloxy)methyl)-4-((2-naphthylmethyl)oxy)piperidine; With boron trichloride; In hexane; dichloromethane; at 0 - 20 ℃; Inert atmosphere;

In methanol; hexane; dichloromethane; Inert atmosphere;
DOI:10.1002/chem.201202374