1,2,7,8,9,10,15,16-octamethyl-3,6,11,14-tetraphenyltetraphospholo[1,2-b;2',1'-d;1'',2''-f;2''',1'''-h][1,2,5,6]tetraphosphocin

Base Information

Chemical Name:1,2,7,8,9,10,15,16-octamethyl-3,6,11,14-tetraphenyltetraphospholo[1,2-b;2',1'-d;1'',2''-f;2''',1'''-h][1,2,5,6]tetraphosphocin
CAS No.:80737-80-0
Molecular Formula:C₄₈H₄₄P₄
Molecular Weight:744.772
Hs Code.:

Synonyms:1,2,7,8,9,10,15,16-octamethyl-3,6,11,14-tetraphenyltetraphospholo[1,2-b;2',1'-d;1'',2''-f;2''',1'''-h][1,2,5,6]tetraphosphocin

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Chemical Property of 1,2,7,8,9,10,15,16-octamethyl-3,6,11,14-tetraphenyltetraphospholo[1,2-b;2',1'-d;1'',2''-f;2''',1'''-h][1,2,5,6]tetraphosphocin

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Technology Process of 1,2,7,8,9,10,15,16-octamethyl-3,6,11,14-tetraphenyltetraphospholo[1,2-b;2',1'-d;1'',2''-f;2''',1'''-h][1,2,5,6]tetraphosphocin

There total 3 articles about 1,2,7,8,9,10,15,16-octamethyl-3,6,11,14-tetraphenyltetraphospholo[1,2-b;2',1'-d;1'',2''-f;2''',1'''-h][1,2,5,6]tetraphosphocin which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 45.0%

: 30540-36-4
3,4-dimethyl-1-phenylphosphole

: 80737-80-0
1,2,7,8,9,10,15,16-octamethyl-3,6,11,14-tetraphenyltetraphospholo[1,2-b;2',1'-d;1'',2''-f;2''',1'''-h][1,2,5,6]tetraphosphocin

Guidance literature:: With 4-bromo-N,N-dimethylaniline; at 180 ℃; for 18h;
DOI:10.1021/ja00087a017

Reference yield:

: 732219-50-0
5,5'-diphenyl-3,3',4,4'-tetramethyl-2,2'-biphosphole

: 80737-80-0
1,2,7,8,9,10,15,16-octamethyl-3,6,11,14-tetraphenyltetraphospholo[1,2-b;2',1'-d;1'',2''-f;2''',1'''-h][1,2,5,6]tetraphosphocin

Guidance literature:: In neat (no solvent); at 170 ℃; for 18h;

Reference yield:

: 137006-41-8
C₂₄H₂₂P₂^(2-)*2Na⁽¹⁺⁾

: 80737-80-0
1,2,7,8,9,10,15,16-octamethyl-3,6,11,14-tetraphenyltetraphospholo[1,2-b;2',1'-d;1'',2''-f;2''',1'''-h][1,2,5,6]tetraphosphocin

Guidance literature:: Multi-step reaction with 2 steps

1: 10 percent / HOAc, H₂O / tetrahydrofuran / -20 deg C to RT

2: neat (no solvent) / 18 h / 170 °C

With water; acetic acid; In tetrahydrofuran;