[1-(4-Carbamimidoyl-benzyl)-2-oxo-2-piperidin-1-yl-ethyl]-carbamic acid benzyl ester; hydriodide

Base Information

Chemical Name:[1-(4-Carbamimidoyl-benzyl)-2-oxo-2-piperidin-1-yl-ethyl]-carbamic acid benzyl ester; hydriodide
CAS No.:101514-68-5
Molecular Formula:C₂₃H₂₈N₄O₃*HI
Molecular Weight:536.413
Hs Code.:

Synonyms:[1-(4-Carbamimidoyl-benzyl)-2-oxo-2-piperidin-1-yl-ethyl]-carbamic acid benzyl ester; hydriodide

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Chemical Property of [1-(4-Carbamimidoyl-benzyl)-2-oxo-2-piperidin-1-yl-ethyl]-carbamic acid benzyl ester; hydriodide

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Technology Process of [1-(4-Carbamimidoyl-benzyl)-2-oxo-2-piperidin-1-yl-ethyl]-carbamic acid benzyl ester; hydriodide

There total 8 articles about [1-(4-Carbamimidoyl-benzyl)-2-oxo-2-piperidin-1-yl-ethyl]-carbamic acid benzyl ester; hydriodide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.0%

: 101514-64-1
4-(2-Benzyloxycarbonylamino-3-oxo-3-piperidin-1-yl-propyl)-thiobenzimidic acid methyl ester; hydriodide

: 101514-68-5
[1-(4-Carbamimidoyl-benzyl)-2-oxo-2-piperidin-1-yl-ethyl]-carbamic acid benzyl ester; hydriodide

Guidance literature:: With ammonium acetate; In methanol; at 60 ℃; for 3h;

Reference yield:

: 110-89-4
piperidine

: 101514-68-5
[1-(4-Carbamimidoyl-benzyl)-2-oxo-2-piperidin-1-yl-ethyl]-carbamic acid benzyl ester; hydriodide

Guidance literature:: Multi-step reaction with 4 steps

1: 90 percent / pyridine / 12 h / Ambient temperature

2: 95 percent / H₂S (gas), TEA / pyridine / 48 h / Ambient temperature

3: 75 percent / acetone / 0.17 h / Heating

4: 85 percent / CH₃CO₂NH₄ / methanol / 3 h / 60 °C

With pyridine; TEA; hydrogen sulfide; ammonium acetate; In pyridine; methanol; acetone;

Reference yield:

: 501-53-1,94274-21-2
benzyl chloroformate

: 101514-68-5
[1-(4-Carbamimidoyl-benzyl)-2-oxo-2-piperidin-1-yl-ethyl]-carbamic acid benzyl ester; hydriodide

Guidance literature:: Multi-step reaction with 6 steps

1: 85 percent / NaOH

2: 85 percent / DDC / pyridine / 1.) 2 h, 2.) room temp., 1 d

3: 90 percent / pyridine / 12 h / Ambient temperature

4: 95 percent / H₂S (gas), TEA / pyridine / 48 h / Ambient temperature

5: 75 percent / acetone / 0.17 h / Heating

6: 85 percent / CH₃CO₂NH₄ / methanol / 3 h / 60 °C

With pyridine; sodium hydroxide; TEA; hydrogen sulfide; ammonium acetate; 2`,3`-dideoxycytidine; In pyridine; methanol; acetone;