tert-butyl (2S)-4,4,4-trichloro-3-hydroxy-1-phenylbutan-2-yl carbamate

Base Information

Chemical Name:tert-butyl (2S)-4,4,4-trichloro-3-hydroxy-1-phenylbutan-2-yl carbamate
CAS No.:1050443-38-3
Molecular Formula:C₁₅H₂₀Cl₃NO₃
Molecular Weight:368.688
Hs Code.:

Synonyms:tert-butyl (2S)-4,4,4-trichloro-3-hydroxy-1-phenylbutan-2-yl carbamate

Suppliers and Price of tert-butyl (2S)-4,4,4-trichloro-3-hydroxy-1-phenylbutan-2-yl carbamate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of tert-butyl (2S)-4,4,4-trichloro-3-hydroxy-1-phenylbutan-2-yl carbamate

Chemical Property:

Purity/Quality:

Safty Information:

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Hazard Codes:

MSDS Files:: SDS file from LookChem

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Technology Process of tert-butyl (2S)-4,4,4-trichloro-3-hydroxy-1-phenylbutan-2-yl carbamate

There total 1 articles about tert-butyl (2S)-4,4,4-trichloro-3-hydroxy-1-phenylbutan-2-yl carbamate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 91.0%

: 650-51-1
sodium trichloroacetate

: 72155-45-4
Boc-L-phenylalaninal

: 1050443-38-3
tert-butyl (2S)-4,4,4-trichloro-3-hydroxy-1-phenylbutan-2-yl carbamate

Guidance literature:: With trichloroacetic acid; In N,N-dimethyl-formamide; at 0 - 20 ℃;
DOI:10.1021/ol8016484

Reference yield:

: 1050443-38-3
tert-butyl (2S)-4,4,4-trichloro-3-hydroxy-1-phenylbutan-2-yl carbamate

: 51871-62-6
(S)-3-tert-butoxycarbonylamino-4-phenylbutanoic acid

Guidance literature:: tert-butyl (2S)-4,4,4-trichloro-3-hydroxy-1-phenylbutan-2-yl carbamate; With sodium tetrahydroborate; diphenyl diselenide; In ethanol; Inert atmosphere;

With sodium hydroxide; In ethanol; at 40 ℃; for 33h; Inert atmosphere;
DOI:10.1021/ol8016484