(2E,7S,8E,10S,11S)-7-{[tert-butyl(dimethyl)silyl]oxy}-10-{[tert-butyl(diphenyl)silyl]oxy}-11-carbamoyloxypentadeca-2,8,14-trienoic acid 1'-(3''-iodo-2''-methylallyl)-4'-methoxycarbonyl-2'-methylpent-3'-enyl ester

Base Information

Chemical Name:(2E,7S,8E,10S,11S)-7-{[tert-butyl(dimethyl)silyl]oxy}-10-{[tert-butyl(diphenyl)silyl]oxy}-11-carbamoyloxypentadeca-2,8,14-trienoic acid 1'-(3''-iodo-2''-methylallyl)-4'-methoxycarbonyl-2'-methylpent-3'-enyl ester
CAS No.:1196064-36-4
Molecular Formula:C₅₀H₇₄INO₈Si₂
Molecular Weight:1000.21
Hs Code.:

(2E,7S,8E,10S,11S)-7-{[tert-butyl(dimethyl)silyl]oxy}-10-{[tert-butyl(diphenyl)silyl]oxy}-11-carbamoyloxypentadeca-2,8,14-trienoic acid 1'-(3''-iodo-2''-methylallyl)-4'-methoxycarbonyl-2'-methylpent-3'-enyl ester

Synonyms:(2E,7S,8E,10S,11S)-7-{[tert-butyl(dimethyl)silyl]oxy}-10-{[tert-butyl(diphenyl)silyl]oxy}-11-carbamoyloxypentadeca-2,8,14-trienoic acid 1'-(3''-iodo-2''-methylallyl)-4'-methoxycarbonyl-2'-methylpent-3'-enyl ester

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Chemical Property of (2E,7S,8E,10S,11S)-7-{[tert-butyl(dimethyl)silyl]oxy}-10-{[tert-butyl(diphenyl)silyl]oxy}-11-carbamoyloxypentadeca-2,8,14-trienoic acid 1'-(3''-iodo-2''-methylallyl)-4'-methoxycarbonyl-2'-methylpent-3'-enyl ester

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Technology Process of (2E,7S,8E,10S,11S)-7-{[tert-butyl(dimethyl)silyl]oxy}-10-{[tert-butyl(diphenyl)silyl]oxy}-11-carbamoyloxypentadeca-2,8,14-trienoic acid 1'-(3''-iodo-2''-methylallyl)-4'-methoxycarbonyl-2'-methylpent-3'-enyl ester

There total 1 articles about (2E,7S,8E,10S,11S)-7-{[tert-butyl(dimethyl)silyl]oxy}-10-{[tert-butyl(diphenyl)silyl]oxy}-11-carbamoyloxypentadeca-2,8,14-trienoic acid 1'-(3''-iodo-2''-methylallyl)-4'-methoxycarbonyl-2'-methylpent-3'-enyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 92.0%

: 1196064-23-9
methyl (2E,4R,5R,7E)-5-{2-[(diethoxy)phosphoryl]acetoxy}-8-iodo-2,4,7-trimethylocta-2,7-dienoate

: 1196064-33-1
carbamic acid (1S,2S,3E,5S)-1-but-3-enyl-5-{[tert-butyl(dimethyl)silyl]oxy}-2-{[tert-butyl(diphenyl)silyl]oxy}-9-oxonon-3-enyl ester

: 1196064-36-4
(2E,7S,8E,10S,11S)-7-{[tert-butyl(dimethyl)silyl]oxy}-10-{[tert-butyl(diphenyl)silyl]oxy}-11-carbamoyloxypentadeca-2,8,14-trienoic acid 1'-(3''-iodo-2''-methylallyl)-4'-methoxycarbonyl-2'-methylpent-3'-enyl ester

Guidance literature:: With N-ethyl-N,N-diisopropylamine; lithium chloride; In acetonitrile; at 20 ℃; for 5h; Inert atmosphere;
DOI:10.1055/s-0029-1216921

Reference yield: 81.0%

: 1196064-36-4
(2E,7S,8E,10S,11S)-7-{[tert-butyl(dimethyl)silyl]oxy}-10-{[tert-butyl(diphenyl)silyl]oxy}-11-carbamoyloxypentadeca-2,8,14-trienoic acid 1'-(3''-iodo-2''-methylallyl)-4'-methoxycarbonyl-2'-methylpent-3'-enyl ester

: 1196064-35-3
C₅₀H₇₃NO₈Si₂

Guidance literature:: With palladium diacetate; caesium carbonate; triethylamine; In N,N-dimethyl-formamide; at 20 ℃; Inert atmosphere;
DOI:10.1055/s-0029-1216921