methyl 2-deoxy-3,4-O-isopropylidene-2-[(9-phenyl-9-fluorenyl)-amino]-D-mannonate

Base Information

• Chemical Name: methyl 2-deoxy-3,4-O-isopropylidene-2-[(9-phenyl-9-fluorenyl)-amino]-D-mannonate
• CAS No.: 154494-79-8
• Molecular Formula: C₂₉H₃₁NO₆
• Molecular Weight: 489.568

Synonyms:methyl 2-deoxy-3,4-O-isopropylidene-2-[(9-phenyl-9-fluorenyl)-amino]-D-mannonate

Chemical Property of methyl 2-deoxy-3,4-O-isopropylidene-2-[(9-phenyl-9-fluorenyl)-amino]-D-mannonate

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Technology Process of methyl 2-deoxy-3,4-O-isopropylidene-2-[(9-phenyl-9-fluorenyl)-amino]-D-mannonate

There total 1 articles about methyl 2-deoxy-3,4-O-isopropylidene-2-[(9-phenyl-9-fluorenyl)-amino]-D-mannonate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

methyl 2-[(9-phenylfluoren-9-yl)amino]-2-deoxy-3,4:5,6-di-O-isopropylidene-D-mannonate (133473-09-3) → methyl 2-deoxy-3,4-O-isopropylidene-2-[(9-phenyl-9-fluorenyl)-amino]-D-mannonate (154494-79-8)

Guidance literature:

With Dowex 50W-X₈ (110 W/Wpercent); In methanol; water; for 32h; Ambient temperature;

DOI:10.1016/0040-4039(94)88373-4

Reference yield: 60.0%

methyl 2-deoxy-3,4-O-isopropylidene-2-[(9-phenyl-9-fluorenyl)-amino]-D-mannonate (154494-79-8) → (S)-Hydroxy-{(4R,5R)-5-[(S)-methoxycarbonyl-(9-phenyl-9H-fluoren-9-ylamino)-methyl]-2,2-dimethyl-[1,3]dioxolan-4-yl}-acetic acid (1054653-92-7)

Guidance literature:

With oxygen; platinum; In water; ethyl acetate; isopropyl alcohol; at 40 ℃;

DOI:10.1021/jo00081a019

Reference yield:

methyl 2-deoxy-3,4-O-isopropylidene-2-[(9-phenyl-9-fluorenyl)-amino]-D-mannonate (154494-79-8) → (S)-((4R,5S)-5-Formyl-2,2-dimethyl-[1,3]dioxolan-4-yl)-(9-phenyl-9H-fluoren-9-ylamino)-acetic acid methyl ester

Guidance literature:

With sodium periodate; In ethanol; for 2h;

DOI:10.1039/a803342k

upstream raw materials:

methyl 2-[(9-phenylfluoren-9-yl)amino]-2-deoxy-3,4:5,6-di-O-isopropylidene-D-mannonate

Downstream raw materials:

(S)-Hydroxy-{(4R,5R)-5-[(S)-methoxycarbonyl-(9-phenyl-9H-fluoren-9-ylamino)-methyl]-2,2-dimethyl-[1,3]dioxolan-4-yl}-acetic acid

methyl 2-deoxy-3,4-O-isopropylidene-2-[(9-phenyl-9-fluorenyl)-amino]-D-lyxonate

methyl 2-deoxy-3,4-O-isopropylidene-5-O-methanesulfonyl-2-[(9-phenyl-9-fluorenyl)-amino]-D-lyxonate

trans-3-hydroxy-1-(9-phenyl-9-fluorenyl)-L-prolinol

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