tert-butyl (2S,3S)-1-hydroxy-3-(4-(trifluoromethyl)phenyl)butan-2-ylcarbamate.

Base Information

Chemical Name:tert-butyl (2S,3S)-1-hydroxy-3-(4-(trifluoromethyl)phenyl)butan-2-ylcarbamate.
CAS No.:944805-05-4
Molecular Formula:C₁₆H₂₂F₃NO₃
Molecular Weight:333.351
Hs Code.:

Synonyms:tert-butyl (2S,3S)-1-hydroxy-3-(4-(trifluoromethyl)phenyl)butan-2-ylcarbamate.

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of tert-butyl (2S,3S)-1-hydroxy-3-(4-(trifluoromethyl)phenyl)butan-2-ylcarbamate.

Chemical Property:

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Technology Process of tert-butyl (2S,3S)-1-hydroxy-3-(4-(trifluoromethyl)phenyl)butan-2-ylcarbamate.

There total 2 articles about tert-butyl (2S,3S)-1-hydroxy-3-(4-(trifluoromethyl)phenyl)butan-2-ylcarbamate. which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 84.0%

: 944805-04-3
tert-butyl (2S,3S)-1-(tert-butyldimethylsilyloxy)-3-(4-(trifluoromethyl)phenyl)butan-2-ylcarbarnate

: 944805-05-4
tert-butyl (2S,3S)-1-hydroxy-3-(4-(trifluoromethyl)phenyl)butan-2-ylcarbamate.

Guidance literature:: With tetrabutyl ammonium fluoride; In tetrahydrofuran; diethyl ether; at 0 ℃; for 1h;

Reference yield: 66.0%

: 944805-16-7
tert-butyl (2S,3S)-1-oxo-1-((R)-2-oxo-4-phenyloxazolidin-3-yl)-3-(4-(trifluoromethyl)phenyl)butan-2-ylcarbamate

: 944805-05-4
tert-butyl (2S,3S)-1-hydroxy-3-(4-(trifluoromethyl)phenyl)butan-2-ylcarbamate.

Guidance literature:: With lithium borohydride; water; In diethyl ether; for 12h;

Reference yield:

: 944805-05-4
tert-butyl (2S,3S)-1-hydroxy-3-(4-(trifluoromethyl)phenyl)butan-2-ylcarbamate.

: 944805-06-5
(R),(S)-tert-butyl 4-((S)-1-(4-(trifluoromethyl)phenyI)-1-S-ethyI)-1,2,3-oxathiazolidine-3-carboxylate, 2-oxide

: (R)-tert-butyl 4-((S)-1-(4-(trifluoromethyl)phenyl)-1-ethyl)-1,2,3-oxathiazolidine-3-carboxylate, 2-oxide

Guidance literature:: tert-butyl (2S,3S)-1-hydroxy-3-(4-(trifluoromethyl)phenyl)butan-2-ylcarbamate.; With thionyl chloride; In acetonitrile; for 0.166667h;

With pyridine; In acetonitrile; at -60 - 20 ℃;