C₂₄H₂₅FIN₃O₄

Base Information

Chemical Name:C₂₄H₂₅FIN₃O₄
CAS No.:1449278-74-3
Molecular Formula:C₂₄H₂₅FIN₃O₄
Molecular Weight:565.383
Hs Code.:

C<sub>24</sub>H<sub>25</sub>FIN<sub>3</sub>O<sub>4</sub>

Synonyms:C₂₄H₂₅FIN₃O₄

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of C₂₄H₂₅FIN₃O₄

Chemical Property:

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Technology Process of C₂₄H₂₅FIN₃O₄

There total 11 articles about C₂₄H₂₅FIN₃O₄ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 45.0%

: 24424-99-5
di-tert-butyl dicarbonate

: 1449278-73-2
C₁₄H₉FIN₃

: 1449278-74-3
C₂₄H₂₅FIN₃O₄

Guidance literature:: With dmap; N-ethyl-N,N-diisopropylamine; In dichloromethane; at 20 ℃; Inert atmosphere;

Reference yield:

: 1449277-90-0
ethyl 8-amino-2-(3-fluorophenyl)-1,7-naphthyridine-5-carboxylate

: 1449278-74-3
C₂₄H₂₅FIN₃O₄

Guidance literature:: Multi-step reaction with 3 steps

1: water; sodium hydroxide / methanol / 2 h / 50 °C / Inert atmosphere

2: N-iodo-succinimide; [bis(acetoxy)iodo]benzene / acetonitrile; water / 0.67 h / 60 °C / Inert atmosphere

3: dmap; N-ethyl-N,N-diisopropylamine / dichloromethane / 20 °C / Inert atmosphere

With dmap; N-iodo-succinimide; [bis(acetoxy)iodo]benzene; water; N-ethyl-N,N-diisopropylamine; sodium hydroxide; In methanol; dichloromethane; water; acetonitrile;

Reference yield:

: 1449278-46-9
5-bromo-7-(2-trimethylsilylethoxymethyl)-1,7-naphthyridin-8-one

: 1449278-74-3
C₂₄H₂₅FIN₃O₄

Guidance literature:: Multi-step reaction with 10 steps

1.1: potassium carbonate; N,N-dimethyl-formamide; palladium diacetate; 1,3-bis(dicyclohexylphosphine)propane / 3 h / 85 °C

2.1: urea hydrogen peroxide adduct / dichloromethane / 0.08 h / 20 °C / Inert atmosphere

2.2: 0.5 h / 20 °C / Inert atmosphere

3.1: oxalyl dichloride / dichloromethane / 0.5 h / 20 °C / Inert atmosphere

4.1: bis(di-tert-?butyl(4-?dimethylaminophenyl)?phosphine)?dichloropalladium(II); potassium phosphate / 1,4-dioxane; water / Inert atmosphere

5.1: tetrabutyl ammonium fluoride / tetrahydrofuran / 2 h / 20 °C / Inert atmosphere

6.1: trichlorophosphate / 3 h / 100 °C / Inert atmosphere

7.1: ammonia / isopropyl alcohol / 1.33 h / 140 °C / Inert atmosphere; Microwave irradiation

8.1: water; sodium hydroxide / methanol / 2 h / 50 °C / Inert atmosphere

9.1: N-iodo-succinimide; [bis(acetoxy)iodo]benzene / acetonitrile; water / 0.67 h / 60 °C / Inert atmosphere

10.1: dmap; N-ethyl-N,N-diisopropylamine / dichloromethane / 20 °C / Inert atmosphere

With dmap; potassium phosphate; N-iodo-succinimide; oxalyl dichloride; [bis(acetoxy)iodo]benzene; bis(di-tert-?butyl(4-?dimethylaminophenyl)?phosphine)?dichloropalladium(II); 1,3-bis(dicyclohexylphosphine)propane; tetrabutyl ammonium fluoride; ammonia; water; palladium diacetate; urea hydrogen peroxide adduct; potassium carbonate; N-ethyl-N,N-diisopropylamine; N,N-dimethyl-formamide; sodium hydroxide; trichlorophosphate; In tetrahydrofuran; 1,4-dioxane; methanol; dichloromethane; water; isopropyl alcohol; acetonitrile;