C₄₂H₅₀IN₂O₇P

Base Information

Chemical Name:C₄₂H₅₀IN₂O₇P
CAS No.:1571072-98-4
Molecular Formula:C₄₂H₅₀IN₂O₇P
Molecular Weight:852.746
Hs Code.:

C<sub>42</sub>H<sub>50</sub>IN<sub>2</sub>O<sub>7</sub>P

Synonyms:C₄₂H₅₀IN₂O₇P

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Chemical Property of C₄₂H₅₀IN₂O₇P

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Technology Process of C₄₂H₅₀IN₂O₇P

There total 6 articles about C₄₂H₅₀IN₂O₇P which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 70.0%

: 1571073-02-3
C₃₃H₃₃IO₆

: 124482-92-4,89992-70-1
2-cyanoethyl-N,N-(diisopropylamino)chlorophosphine

: 1571072-98-4
C₄₂H₅₀IN₂O₇P

Guidance literature:: With N-ethyl-N,N-diisopropylamine; In dichloromethane; at 0 - 20 ℃; for 3h; Inert atmosphere;
DOI:10.1021/jo4028227

Reference yield:

: 173327-56-5
3,5-bis-O,O-(tert-butyldimethylsilyl)-1,2-didehydro-1,2-dideoxy-D-ribofuranose

: 1571072-98-4
C₄₂H₅₀IN₂O₇P

Guidance literature:: Multi-step reaction with 6 steps

1: tributyl-amine; palladium diacetate; triphenyl-arsane / N,N-dimethyl-formamide / 15 h / 70 °C / Inert atmosphere

2: tetrabutyl ammonium fluoride / N,N-dimethyl-formamide; tetrahydrofuran / 1.5 h / 0 °C / Inert atmosphere

3: sodium tris(acetoxy)borohydride / acetic acid; acetonitrile / 1 h / 0 °C / Inert atmosphere

4: sodium iodide; N,N’-trans-dimethyl cyclohexane-1,2-diamine / pentan-1-ol / 3 h / 130 °C / Inert atmosphere

5: pyridine / 16 h / 20 °C / Inert atmosphere

6: N-ethyl-N,N-diisopropylamine / dichloromethane / 3 h / 0 - 20 °C / Inert atmosphere

With pyridine; tributyl-amine; triphenyl-arsane; tetrabutyl ammonium fluoride; palladium diacetate; sodium tris(acetoxy)borohydride; N-ethyl-N,N-diisopropylamine; sodium iodide; N,N’-trans-dimethyl cyclohexane-1,2-diamine; In tetrahydrofuran; dichloromethane; pentan-1-ol; acetic acid; N,N-dimethyl-formamide; acetonitrile;
DOI:10.1021/jo4028227

Reference yield:

: 1571073-00-1
C₁₂H₁₃BrO₄

: 1571072-98-4
C₄₂H₅₀IN₂O₇P

Guidance literature:: Multi-step reaction with 4 steps

1: sodium tris(acetoxy)borohydride / acetic acid; acetonitrile / 1 h / 0 °C / Inert atmosphere

2: sodium iodide; N,N’-trans-dimethyl cyclohexane-1,2-diamine / pentan-1-ol / 3 h / 130 °C / Inert atmosphere

3: pyridine / 16 h / 20 °C / Inert atmosphere

4: N-ethyl-N,N-diisopropylamine / dichloromethane / 3 h / 0 - 20 °C / Inert atmosphere

With pyridine; sodium tris(acetoxy)borohydride; N-ethyl-N,N-diisopropylamine; sodium iodide; N,N’-trans-dimethyl cyclohexane-1,2-diamine; In dichloromethane; pentan-1-ol; acetic acid; acetonitrile;
DOI:10.1021/jo4028227