4-[2-(1H-benzoimidazol-2-ylmethanesulfonyl)-1-hydroxy-ethyl]-2,6-di-tert-butyl-phenol

Base Information

Chemical Name:4-[2-(1H-benzoimidazol-2-ylmethanesulfonyl)-1-hydroxy-ethyl]-2,6-di-tert-butyl-phenol
CAS No.:639494-52-3
Molecular Formula:C₂₄H₃₂N₂O₄S
Molecular Weight:444.595
Hs Code.:

4-[2-(1<i>H</i>-benzoimidazol-2-ylmethanesulfonyl)-1-hydroxy-ethyl]-2,6-di-<i>tert</i>-butyl-phenol

Synonyms:4-[2-(1H-benzoimidazol-2-ylmethanesulfonyl)-1-hydroxy-ethyl]-2,6-di-tert-butyl-phenol

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 4-[2-(1H-benzoimidazol-2-ylmethanesulfonyl)-1-hydroxy-ethyl]-2,6-di-tert-butyl-phenol

Chemical Property:

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Technology Process of 4-[2-(1H-benzoimidazol-2-ylmethanesulfonyl)-1-hydroxy-ethyl]-2,6-di-tert-butyl-phenol

There total 4 articles about 4-[2-(1H-benzoimidazol-2-ylmethanesulfonyl)-1-hydroxy-ethyl]-2,6-di-tert-butyl-phenol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1026418-11-0
4-[2-(1H-benzoimidazol-2-ylmethylsulfanyl)-1-hydroxy-ethyl]-2,6-di-tert-butyl-phenol

: 639494-52-3
4-[2-(1H-benzoimidazol-2-ylmethanesulfonyl)-1-hydroxy-ethyl]-2,6-di-tert-butyl-phenol

Guidance literature:: With Oxone; In dichloromethane; water; tert-butyl alcohol; at 20 ℃; for 7h;
DOI:10.1016/S0223-5234(03)00144-2

Reference yield:

: 4344-85-8
(1H-benzimidazol-2-yl)methanethiol

: 639494-52-3
4-[2-(1H-benzoimidazol-2-ylmethanesulfonyl)-1-hydroxy-ethyl]-2,6-di-tert-butyl-phenol

Guidance literature:: Multi-step reaction with 3 steps

1: NaH / dimethylformamide / 2 h / 20 °C

2: NaBH₄ / CHCl₃; methanol / 0.5 h / 20 °C

3: potassium mono persulphate triple salt / CH₂Cl₂; 2-methyl-propan-2-ol; H₂O / 7 h / 20 °C

With Oxone; sodium tetrahydroborate; sodium hydride; In methanol; dichloromethane; chloroform; water; N,N-dimethyl-formamide; tert-butyl alcohol;
DOI:10.1016/S0223-5234(03)00144-2

Reference yield:

: 95-54-5
1,2-diamino-benzene

: 639494-52-3
4-[2-(1H-benzoimidazol-2-ylmethanesulfonyl)-1-hydroxy-ethyl]-2,6-di-tert-butyl-phenol

Guidance literature:: Multi-step reaction with 4 steps

1: HCl / 5 h / Heating

2: NaH / dimethylformamide / 2 h / 20 °C

3: NaBH₄ / CHCl₃; methanol / 0.5 h / 20 °C

4: potassium mono persulphate triple salt / CH₂Cl₂; 2-methyl-propan-2-ol; H₂O / 7 h / 20 °C

With hydrogenchloride; Oxone; sodium tetrahydroborate; sodium hydride; In methanol; dichloromethane; chloroform; water; N,N-dimethyl-formamide; tert-butyl alcohol;
DOI:10.1016/S0223-5234(03)00144-2