S- (Phenyl)thioacetate

Base Information

• Chemical Name: S- (Phenyl)thioacetate
• CAS No.: 145235-52-5
• Molecular Formula: C₂₀H₂₀N₂O₃S
• Molecular Weight: 368.456

Synonyms:S- (Phenyl)thioacetate

Chemical Property of S- (Phenyl)thioacetate

Chemical Property:

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Technology Process of S- (Phenyl)thioacetate

There total 1 articles about S- (Phenyl)thioacetate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

S- (Phenyl)thioacetate (145235-51-4) → S- (Phenyl)thioacetate (145235-52-5)

Guidance literature:

With potassium perchlorate; trifluoroacetic acid; at 25 ℃; for 1h;

DOI:10.1002/hlca.19920750610

Reference yield: 60.0%

Dibenzyl 2,3-Dibromosuccinate (145235-54-7) + S- (Phenyl)thioacetate (145235-52-5) → Dibenzyl (6RS,7RS)-8-Oxo-7-(phenylacetamido)-4-thia-1-azabicyclo<4.2.0>octane-2,3-dicarboxylate (145235-55-8)

Guidance literature:

With piperidine; In N,N-dimethyl-formamide; at 80 ℃; for 3.5h;

DOI:10.1002/hlca.19920750610

Reference yield: 45.0%

Benzyl Dibromoacetate (64503-07-7) + S- (Phenyl)thioacetate (145235-52-5) → Benzyl (2RS,5SR,6SR)-7-Oxo-6-(phenylacetamido)-3-thia-1-azabicyclo<3.2.0>heptane-2-carboxylate (69284-21-5,145307-13-7)

Guidance literature:

With piperidine; In tert-butyl alcohol; for 2h; Heating;

DOI:10.1002/hlca.19920750610

upstream raw materials:

S- (Phenyl)thioacetate

Downstream raw materials:

Dibenzyl (6RS,7RS)-8-Oxo-7-(phenylacetamido)-4-thia-1-azabicyclo<4.2.0>octane-2,3-dicarboxylate

Benzyl (2RS,5SR,6SR)-7-Oxo-6-(phenylacetamido)-3-thia-1-azabicyclo<3.2.0>heptane-2-carboxylate

(2RS,5SR,6SR)-7-Oxo-6-(phenylacetamido)-3-thia-1-azabicyclo<3.2.0>heptane-2-carboxylic Acid

(6RS,7RS)-8-Oxo-7-(phenylacetamido)-4-thia-1-azabicyclo<4.2.0>oct-2-ene-2,3-dicarboxylate

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