N-[(1S,2R)-2-(3,5-dihydroxybenzamido)cyclohexanecarboxy]-α-L-fucopyranosylamine

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Chemical Name:N-[(1S,2R)-2-(3,5-dihydroxybenzamido)cyclohexanecarboxy]-α-L-fucopyranosylamine
CAS No.:1329602-77-8
Molecular Formula:C₂₀H₂₈N₂O₈
Molecular Weight:424.451
Hs Code.:

Synonyms:N-[(1S,2R)-2-(3,5-dihydroxybenzamido)cyclohexanecarboxy]-α-L-fucopyranosylamine

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of N-[(1S,2R)-2-(3,5-dihydroxybenzamido)cyclohexanecarboxy]-α-L-fucopyranosylamine

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Technology Process of N-[(1S,2R)-2-(3,5-dihydroxybenzamido)cyclohexanecarboxy]-α-L-fucopyranosylamine

There total 2 articles about N-[(1S,2R)-2-(3,5-dihydroxybenzamido)cyclohexanecarboxy]-α-L-fucopyranosylamine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

: 1352809-42-7
C₃₀H₃₈N₂O₁₃

: 1329602-77-8
N-[(1S,2R)-2-(3,5-dihydroxybenzamido)cyclohexanecarboxy]-α-L-fucopyranosylamine

Guidance literature:: With methanol; sodium methylate; at 20 ℃; Inert atmosphere;
DOI:10.1039/c1ob05573a

Reference yield:

: C₁₉H₂₉NO₉

: 35354-29-1
3,5-diacetoxybenzoic acid

: 1329602-77-8
N-[(1S,2R)-2-(3,5-dihydroxybenzamido)cyclohexanecarboxy]-α-L-fucopyranosylamine

Guidance literature:: Multi-step reaction with 2 steps

1: O-(1H-benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium hexafluorophosphate; triethylamine / dichloromethane / 18 h / 20 °C / Inert atmosphere

2: methanol; sodium methylate / 20 °C / Inert atmosphere

With methanol; sodium methylate; O-(1H-benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium hexafluorophosphate; triethylamine; In dichloromethane; 2: Zemplen deprotection;
DOI:10.1039/c1ob05573a